Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers)

Base Information

Chemical Name:Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers)
CAS No.:101084-46-2
Molecular Formula:C₆H₁₀I₂O₂
Molecular Weight:367.953
Hs Code.:
Mol file:101084-46-2.mol

Synonyms:Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers);2,5-Bis(iodoMethyl)-p-dioxane;2,5-Bis(iodomethyl)-1,4-dioxane

Suppliers and Price of Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
Bis(2,5-iodomethyl)dioxane(MixtureofDiastereomers)
5g
$ 1110.00

TRC
Bis(2,5-iodomethyl)dioxane(MixtureofDiastereomers)
500mg
$ 140.00

Total 4 raw suppliers

Chemical Property of Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers)

Chemical Property:

PSA：18.46000
LogP:1.64040
Storage Temp.:Refrigerator
Solubility.:Chloroform, Ethyl Acetate

Purity/Quality:

98%min ^*data from raw suppliers

Bis(2,5-iodomethyl)dioxane(MixtureofDiastereomers) ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Uses A derivative of dioxane.

Technology Process of Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers)

There total 7 articles about Bis(2,5-iodomethyl)dioxane (Mixture of Diastereomers) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 107-18-6
allyl alcohol

: 624-57-7
epiiodohydrin

: 56127-59-4
trans-2,6-Bis(iodomethyl)-1,4-dioxane

: 56127-59-4,101084-46-2,121137-93-7,121137-94-8
cis-2,6-Bis(iodomethyl)-1,4-dioxane

Guidance literature:: With iodonium(di-γ-collidine) perchlorate; In dichloromethane; at 20 ℃; for 1.5h;
DOI:10.1055/s-1988-27731

Reference yield:

: 6938-88-1
(+/-)-cis-[1,4]dioxane-2,5-dicarboxylic acid

: 56127-59-4,101084-46-2,121137-93-7,121137-94-8
cis-2,6-Bis(iodomethyl)-1,4-dioxane

Guidance literature:: Multi-step reaction with 4 steps

1: diethyl ether

2: lithium alanate; diethyl ether

3: pyridine

4: acetone; sodium iodide

With pyridine; lithium aluminium tetrahydride; diethyl ether; acetone; sodium iodide;
DOI:10.1021/ja01653a046