1,3-二BOC丙二胺

Base Information

• Chemical Name: 1,3-二BOC丙二胺
• CAS No.: 33105-94-1
• Molecular Formula: C13H26N2O4
• Molecular Weight: 274.35654
• Mol file: 33105-94-1.mol

Synonyms:1,3-二BOC丙二胺;Di-Tert-Butyl propane-1,3-diyldicarbaMate

Chemical Property of 1,3-二BOC丙二胺

Chemical Property:

• Melting Point: 110-111 °C
• Boiling Point: 394.9±25.0 °C(Predicted)
• PKA: 12.46±0.46(Predicted)
• Density: 1.024±0.06 g/cm3(Predicted)

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1,3-二BOC丙二胺

There total 5 articles about 1,3-二BOC丙二胺 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

di-tert-butyl dicarbonate (24424-99-5) + Trimethylenediamine (109-76-2,54018-94-9) → N,N'-di-Boc-1,3-propyldiamine (33105-94-1)

Guidance literature:

In neat (no solvent); at 80 ℃; for 0.166667h; chemoselective reaction; Green chemistry;

DOI:10.1007/s11164-016-2702-9

Reference yield: 96.0%

S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine (41840-28-2) + Trimethylenediamine (109-76-2,54018-94-9) → N,N'-di-Boc-1,3-propyldiamine (33105-94-1)

Guidance literature:

With triethylamine; In 1,4-dioxane; water; for 6h; Ambient temperature;

Reference yield: 93.0%

di-tert-butyl dicarbonate (24424-99-5) + Trimethylenediamine (109-76-2,54018-94-9) → N,N'-di-Boc-1,3-propyldiamine (33105-94-1) + N-Boc-1,3-diaminopropane (75178-96-0)

Guidance literature:

In 1,4-dioxane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2010.02.035

upstream raw materials:

S-tert-butoxycarbonyl-4,6-dimethyl-2-mercaptopyrimidine

Trimethylenediamine

di-tert-butyl dicarbonate

N-(tert-butyloxycarbonyl) azide

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