1-broMo-3-iodo-2-nitrobenzene

Base Information

• Chemical Name: 1-broMo-3-iodo-2-nitrobenzene
• CAS No.: 1126425-84-0
• Molecular Formula: C6H3BrINO2
• Molecular Weight: 327.90199
• Hs Code.: 2904990090
• Mol file: 1126425-84-0.mol

Synonyms:1-broMo-3-iodo-2-nitrobenzene;2-Bromo-6-iodonitrobenzene

Chemical Property of 1-broMo-3-iodo-2-nitrobenzene

Chemical Property:

• Boiling Point: 298.5±30.0 °C(Predicted)
• Density: 2.349±0.06 g/cm3(Predicted)

Purity/Quality:

98.5% ^*data from raw suppliers

1-Bromo-3-iodo-2-nitrobenzene ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-broMo-3-iodo-2-nitrobenzene

There total 2 articles about 1-broMo-3-iodo-2-nitrobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

2-bromo-6-iodobenzenamine (84483-27-2) → 1-bromo-3-iodo-2-nitrobenzene (1126425-84-0)

Guidance literature:

With 3-chloro-benzenecarboperoxoic acid; In 1,2-dichloro-ethane; at 70 ℃; for 2h;

DOI:10.1021/ol8026957

Reference yield:

→ 2-bromo-4-iodo-1-nitro-benzene (860603-83-4) + 1-bromo-3-iodo-2-nitrobenzene (1126425-84-0)

Guidance literature:

With nitric acid; bleibt beim Umkrystallisieren des Rohprodukts in der Mutterlauge;

Reference yield: 76.0%

1-bromo-3-iodo-2-nitrobenzene (1126425-84-0) + benzofurane-3-ylboronic acid → C14H8BrNO3

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In ethanol; water; toluene; at 80 ℃; Inert atmosphere;

upstream raw materials:

2-bromo-6-iodobenzenamine

Downstream raw materials:

1-bromo-9H-carbazole

10-bromo-11H-benzo[a]carbazole

Refernces