3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide

Base Information

Chemical Name:3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide
CAS No.:1059171-45-7
Molecular Formula:C₁₃H₂₀BNO₄S
Molecular Weight:297.183
Hs Code.:

Synonyms:3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide

Suppliers and Price of 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide

There total 2 articles about 3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzenemethanesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 919354-04-4
1-(3-bromophenyl)methanesulfonamide

: 73183-34-3
bis(pinacol)diborane

: 1059171-45-7
1-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanesulfonamide

Guidance literature:: With potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; at 70 ℃; Inert atmosphere;

Reference yield:

: 58236-74-1
(3-bromophenyl)methanesulfonyl chloride

: 1059171-45-7
1-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanesulfonamide

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / 1,4-dioxane; water / -15 - 20 °C

2: potassium acetate / (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride / 1,4-dioxane / 70 °C / Inert atmosphere

With ammonium hydroxide; potassium acetate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water;

Reference yield:

: 1059171-45-7
1-[3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)phenyl]methanesulfonamide

: 1198436-89-3
N-(6-bromo-1H-indazol-4-yl)-2-methyl-1,3-thiazole-4-carboxamide

: 1198803-22-3
N-(6-{3-[(aminosulfonyl)methyl]phenyl}-1H-indazol-4-yl)-2-methyl-1,3-thiazole-4-carboxamide

Guidance literature:: With sodium carbonate; (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; In 1,4-dioxane; water; at 150 ℃; for 0.25h; Microwave irratiation;