5-[Di(1-adaMantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole, 97+% (AdaMantyl-BippyPhos)

Base Information

• Chemical Name: 5-[Di(1-adaMantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole, 97+% (AdaMantyl-BippyPhos)
• CAS No.: 1239478-87-5
• Molecular Formula: C44H47N4P
• Molecular Weight: 662.858
• Mol file: 1239478-87-5.mol

Synonyms:5-[Di(1-adaMantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole, 97+% (AdaMantyl-BippyPhos);5-[Bis(1-adamantyl)phosphino]-1′,3′,5′-triphenyl-1,4′-bi-1H-pyrazole;5-[Di(1-adamantyl)phosphino]-1′,3′,5′-triphenyl-1′H-[1,4′]bipyrazole;Adamantyl-BippyPhos;Ad-BGPhos;5-[Di(1-adamantyl)phosphino]-1',3',5'-triphenyl-1'H-[1,4']bipyrazole 97%

Chemical Property of 5-[Di(1-adaMantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole, 97+% (AdaMantyl-BippyPhos)

Chemical Property:

• Melting Point: 295-300°C
• PKA: -0.58±0.19(Predicted)
• PSA: 49.23000
• LogP: 10.43680
• Storage Temp.: 2-8°C

Purity/Quality:

97+% ^*data from raw suppliers

5-[Di(1-adamantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole ^*data from reagent suppliers

Safty Information:

• Statements: 36/37/38
• Safety Statements: 26-37

MSDS Files:

SDS file from LookChem

Useful:

• Uses: 5-[Di(1-adamantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole can be used as a catalyst. 5-[Di(1-adamantyl)phosphino]-1′,3′,5′-triphenyl-1′H-[1,4′]bipyrazole (Ad-BippyPhos) is an effective ligand that catalyzes C-O coupling reactions of aryl and heteroaryl bromides/chlorides with primary aliphatic alcohols. It can also be used as a catalyst in the synthesis of fluorinated anilines by coupling fluoroalkylamines with aryl bromides and chlorides.

Technology Process of 5-[Di(1-adaMantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole, 97+% (AdaMantyl-BippyPhos)

There total 1 articles about 5-[Di(1-adaMantyl)phosphino](1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole, 97+% (AdaMantyl-BippyPhos) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-(1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole (894085-99-5) + di-1-adamantylchlorophosphane (157282-19-4) → 5-(di(adamantan-1-yl)phosphino)-1′,3′,5′-triphenyl-1′H-1,4′-bipyrazole (1239478-87-5)

Guidance literature:

1-(1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole; With n-butyllithium; In tetrahydrofuran; hexane; cyclohexane; at -78 ℃; for 2.25h;

di-1-adamantylchlorophosphane; In tetrahydrofuran; hexane; cyclohexane; at -30 - 20 ℃;

DOI:10.1021/ja103248d

upstream raw materials:

1-(1,3,5-triphenyl-1H-pyrazol-4-yl)-1H-pyrazole

di-1-adamantylchlorophosphane

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