2,5-Dichloro-4'-nitrobiphenyl

Base Information

Chemical Name:2,5-Dichloro-4'-nitrobiphenyl
CAS No.:2765-22-2
Molecular Formula:C₁₂H₇Cl₂NO₂
Molecular Weight:268.099
Hs Code.:2904909090
DSSTox Substance ID:DTXSID60548918
Nikkaji Number:J80.555F
Wikidata:Q82427773
Mol file:2765-22-2.mol

Synonyms:2765-22-2;2,5-Dichloro-4'-nitrobiphenyl;DTXSID60548918;2,5-Dichloro-4'-nitro-1,1'-biphenyl;1, 4-dichloro-2-(4-nitrophenyl)benzene

Suppliers and Price of 2,5-Dichloro-4'-nitrobiphenyl

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 2,5-Dichloro-4'-nitrobiphenyl

Chemical Property:

PSA：45.82000
LogP:5.09180
XLogP3:5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:1
Exact Mass:266.9853839
Heavy Atom Count:17
Complexity:274

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC=C1C2=C(C=CC(=C2)Cl)Cl)[N+](=O)[O-]

Technology Process of 2,5-Dichloro-4'-nitrobiphenyl

There total 8 articles about 2,5-Dichloro-4'-nitrobiphenyl which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 106-46-7,84348-21-0
para-dichlorobenzene

: 586-78-7
para-nitrophenyl bromide

: 2765-22-2
2'.5'-Dichlor-4-nitro-biphenyl

Guidance literature:: With PdCl(C₃H₅)(1,4-bis(diphenylphosphino)butane); potassium acetate; In N,N-dimethyl acetamide; at 150 ℃; for 20h; regioselective reaction; Inert atmosphere; Schlenk technique;
DOI:10.1039/c3cy00757j

Reference yield: 36.0%

: 106-46-7,84348-21-0
para-dichlorobenzene

: 92722-14-0
tert-butyl 2-(4-nitrophenyl)diazenecarboxylate

: 2765-22-2
2'.5'-Dichlor-4-nitro-biphenyl

Guidance literature:: With manganese(IV) oxide; at 160 ℃;
DOI:10.1021/jo202406k

Reference yield:

: 1354828-66-2
tert-butyl 2-(4-cyanophenyl)diazene-1-carboxylate

: 2765-22-2
2'.5'-Dichlor-4-nitro-biphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane / Inert atmosphere

2: manganese(IV) oxide / 160 °C

With manganese(IV) oxide; In dichloromethane;
DOI:10.1021/jo202406k