(R)-1,3'-Bipyrrolidine dihydrochloride

Base Information

• Chemical Name: (R)-1,3'-Bipyrrolidine dihydrochloride
• CAS No.: 913702-34-8
• Molecular Formula: C₈H₁₆N₂*ClH
• Molecular Weight: 176.689
• Hs Code.: 2933998090
• Mol file: 913702-34-8.mol

Synonyms:(R)-1,3'-Bipyrrolidine dihydrochloride;(3R)-3-(pyrrolidin-1-yl)pyrrolidine dihydrochloride

Chemical Property of (R)-1,3'-Bipyrrolidine dihydrochloride

Chemical Property:

• PSA: 15.27000
• LogP: 2.31480
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

(R)-1,3''-BipyrrolidineDihydrochloride ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (R)-1,3'-Bipyrrolidine dihydrochloride

There total 4 articles about (R)-1,3'-Bipyrrolidine dihydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl (R)-[1,3'-bipyrrolidine]-1'-carboxylate (913702-27-9) → (R)-1,3'-bipyrrolidine dihydrochloride (913702-34-8,957540-36-2)

Guidance literature:

With hydrogenchloride; In 1,4-dioxane; for 2h;

Reference yield: 100.0%

(R)-1'-benzyl-[1,3']bipyrrolidinyl (900164-96-7) → (R)-1,3'-bipyrrolidine dihydrochloride (913702-34-8,957540-36-2)

Guidance literature:

With hydrogenchloride; 10% palladium on carbon; hydrogen; In methanol; water; at 40 ℃; for 24h; under 30003 Torr;

DOI:10.1016/j.tetasy.2010.04.038

Reference yield:

(S)-1-benzyl-3-(1-pyrrolidinyl)pyrrolidine (859213-31-3) → (S)-3-(1-pyrrolidinyl)pyrrolidine hydrochloride (859213-32-4,913702-34-8,957540-36-2)

Guidance literature:

With hydrogenchloride; hydrogen; palladium 10% on activated carbon; In ethanol; water; at 20 ℃; under 760.051 Torr;

upstream raw materials:

(S)-1-benzyl-3-(1-pyrrolidinyl)pyrrolidine

C₁₃H₂₄N₂O₂

(R)-1'-benzyl-[1,3']bipyrrolidinyl

tert-butyl (R)-[1,3'-bipyrrolidine]-1'-carboxylate

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