4-(5-chloro-3-isopropylpyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethylbenzenesulfonamide

Base Information

Chemical Name:4-(5-chloro-3-isopropylpyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethylbenzenesulfonamide
CAS No.:771499-34-4
Molecular Formula:C17H20ClN5O2S
Molecular Weight:393.897
Hs Code.:

Synonyms:4-(5-chloro-3-isopropylpyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethylbenzenesulfonamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 4-(5-chloro-3-isopropylpyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethylbenzenesulfonamide

Chemical Property:

PSA：87.98000
LogP:4.65380

Purity/Quality:

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Technology Process of 4-(5-chloro-3-isopropylpyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethylbenzenesulfonamide

There total 1 articles about 4-(5-chloro-3-isopropylpyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 1709-59-7
4-amino-N,N-dimethylbenzenesulphonamide

: 771510-32-8
5,7-dichloro-3-iso-propyl-pyrazolo[1,5-a]pyrimidine

: 771499-34-4
3-isopropyl-5-chloro-7-[4-(N,N-dimethylsulfonamido)phenylamino]pyrazolo[1,5-a]pyrimidine

Guidance literature:: In ethanol; for 16h; Heating / reflux;

Reference yield:

: 78-83-1
2-methyl-propan-1-ol

: 771499-34-4
3-isopropyl-5-chloro-7-[4-(N,N-dimethylsulfonamido)phenylamino]pyrazolo[1,5-a]pyrimidine

: 4-(5-isobutoxy-3-isopropyl-pyrazolo[1,5-a]pyrimidin-7-ylamino)-N,N-dimethyl-benzenesulfonamide

Guidance literature:: With sodium hydride; triethylamine; In 1,4-dioxane; acetonitrile; at 180 ℃; for 3h; microwave irradiation;
DOI:10.1016/j.bmcl.2004.12.073

Reference yield:

: 3385-21-5,26772-34-9,26883-70-5,115092-57-4
1,3-diaminocyclohexane

: 771499-34-4
3-isopropyl-5-chloro-7-[4-(N,N-dimethylsulfonamido)phenylamino]pyrazolo[1,5-a]pyrimidine

: 4-[5-(3-amino-cyclohexylamino)-3-isopropyl-pyrazolo[1,5-a]pyrimidin-7-ylamino]-N,N-dimethyl-benzenesulfonamide

Guidance literature:: With triethylamine; In 1,4-dioxane; acetonitrile; at 180 ℃; for 3h; microwave irradiation;
DOI:10.1016/j.bmcl.2004.12.073