Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI)

Base Information

Chemical Name:Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI)
CAS No.:199604-18-7
Molecular Formula:C₉H₈FNO₂
Molecular Weight:181.166
Hs Code.:
Mol file:199604-18-7.mol

Synonyms:Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI)

Suppliers and Price of Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemicals and raw materials
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Total 2 raw suppliers

Chemical Property of Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI)

Chemical Property:

Purity/Quality:: 99%+ ^*data from raw suppliers

Safty Information:

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Technology Process of Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI)

There total 2 articles about Carbamic acid, [(4-fluorophenyl)methylene]-, methyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 79-22-1
methyl chloroformate

: 160313-82-6
N-trimethylsilyl-4-fluorobenzaldimine

: 199604-18-7
N-methoxycarbonyl-4-fluorobenzaldimine

Guidance literature:: In chloroform; for 2h; Ambient temperature;
DOI:10.1002/chem.19970031019

Reference yield:

: 459-57-4
4-fluorobenzaldehyde

: 199604-18-7
N-methoxycarbonyl-4-fluorobenzaldimine

Guidance literature:: Multi-step reaction with 2 steps

1: 71 percent / BuLi / hexane; tetrahydrofuran / 1.) 0 deg C, 10 min, 2.) r.t., 1 h

2: 77 percent / CHCl₃ / 2 h / Ambient temperature

With n-butyllithium; In tetrahydrofuran; hexane; chloroform;
DOI:10.1002/chem.19970031019