N-Cyclooctylidenecyclohexanamine

Base Information

• Chemical Name: N-Cyclooctylidenecyclohexanamine
• CAS No.: 54699-42-2
• Molecular Formula: C14H25N
• Molecular Weight: 207.359
• Mol file: 54699-42-2.mol

Synonyms:N-Cyclohexylcyclooctanimine;N-Cyclooctylidenecyclohexanamine

Chemical Property of N-Cyclooctylidenecyclohexanamine

Chemical Property:

• Boiling Point: 80 - 90 °C (0.001 mmHg)
• PSA: 12.36000
• LogP: 4.50440

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-Cyclooctylidenecyclohexanamine

There total 1 articles about N-Cyclooctylidenecyclohexanamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cycloactanone (502-49-8) + cyclohexylmethylamine (3218-02-8) → N-cyclohexyl-N-cyclooctylidenamine (54699-42-2)

Guidance literature:

In toluene; Reflux;

DOI:10.1016/j.bmcl.2012.02.054

Reference yield: 96.0%

triethyl borane (97-94-9) + N-cyclohexyl-N-cyclooctylidenamine (54699-42-2) → ethane (74-84-0) + (N-Cyclohexyl-1-cyclooctenylamino)diethylboran (74810-32-5)

Guidance literature:

With diethylboryl-pivalate; at 150 ℃; for 6h; under 5320 Torr;

Reference yield:

1-iodo-2-(naphth-1-yl)ethane (75325-81-4) + N-cyclohexyl-N-cyclooctylidenamine (54699-42-2) → C26H35N

Guidance literature:

N-cyclohexyl-N-cyclooctylidenamine; With n-butyllithium; diisopropylamine; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h;

1-iodo-2-(naphth-1-yl)ethane; In tetrahydrofuran; hexane; at 0 ℃; for 0.5h; Further stages.;

DOI:10.1002/chem.200700057

upstream raw materials:

cycloactanone

cyclohexylmethylamine

Downstream raw materials:

ethane

(N-Cyclohexyl-1-cyclooctenylamino)diethylboran

1-cyclohexylmethyl-2-oxo-1,2,5,6,7,8,9,10-octahydro-cycloocta[b]pyridine-3-carboxylic acid chloride