2-Iodo-4-methoxy-benzoic acid methyl ester

Base Information

Chemical Name:2-Iodo-4-methoxy-benzoic acid methyl ester
CAS No.:54413-84-2
Molecular Formula:C₉H₉IO₃
Molecular Weight:292.073
Hs Code.:2918999090
Mol file:54413-84-2.mol

Synonyms:2-Iodo-4-methoxy-benzoic acid methyl ester;Methyl 2-iodo-4-methoxybenzoate

Suppliers and Price of 2-Iodo-4-methoxy-benzoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Alichem
Methyl2-iodo-4-methoxybenzoate
10g
$ 603.00

Alichem
Methyl2-iodo-4-methoxybenzoate
25g
$ 1278.36

Alichem
Methyl2-iodo-4-methoxybenzoate
100g
$ 2706.80

Atlantic Research Chemicals
Methyl2-Iodo-4-methoxybenzoate 95%
1gm:
$ 356.99

Crysdot
Methyl2-iodo-4-methoxybenzoate 95+%
10g
$ 419.00

Crysdot
Methyl2-iodo-4-methoxybenzoate 95+%
100g
$ 1880.00

Crysdot
Methyl2-iodo-4-methoxybenzoate 95+%
5g
$ 326.00

Crysdot
Methyl2-iodo-4-methoxybenzoate 95+%
25g
$ 842.00

Matrix Scientific
Methyl 2-iodo-4-methoxybenzoate 97%
1g
$ 623.00

Total 6 raw suppliers

Chemical Property of 2-Iodo-4-methoxy-benzoic acid methyl ester

Chemical Property:

Purity/Quality:

97% ^*data from raw suppliers

Methyl2-iodo-4-methoxybenzoate ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Iodo-4-methoxy-benzoic acid methyl ester

There total 4 articles about 2-Iodo-4-methoxy-benzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 54435-09-5
2-iodo-4-methoxybenzoic acid

: 74-88-4
methyl iodide

: 54413-84-2
methyl 2-iodo-4-methoxybenzoate

Guidance literature:: With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 20 ℃; Inert atmosphere;
DOI:10.1016/j.molstruc.2021.132135

Reference yield:

: 54435-09-5
2-iodo-4-methoxybenzoic acid

: 54413-84-2
methyl 2-iodo-4-methoxybenzoate

Guidance literature:: With sulfuric acid; In methanol; water;

Reference yield:

: 4294-95-5
4-methoxyanthranilic acid

: 54413-84-2
methyl 2-iodo-4-methoxybenzoate

Guidance literature:: Multi-step reaction with 2 steps

1.1: sulfuric acid; sodium nitrite / water / 0 °C / Inert atmosphere

1.2: 70 °C / Inert atmosphere

2.1: 1,8-diazabicyclo[5.4.0]undec-7-ene / acetonitrile / 20 °C / Inert atmosphere

With sulfuric acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium nitrite; In water; acetonitrile; 1.1: |Sandmeyer Reaction;
DOI:10.1016/j.molstruc.2021.132135