2-(2-aMino-5-broMophenyl)-2-oxoacetic acid

Base Information

Chemical Name:2-(2-aMino-5-broMophenyl)-2-oxoacetic acid
CAS No.:120095-19-4
Molecular Formula:C₈H₅BrNO₃*K
Molecular Weight:282.135
Hs Code.:2924299090
Mol file:120095-19-4.mol

Synonyms:2-(2-aMino-5-broMophenyl)-2-oxoacetic acid;potassiuM 2-(2-aMino-5-broMophenyl)-2-oxoacetate

Suppliers and Price of 2-(2-aMino-5-broMophenyl)-2-oxoacetic acid

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
Potassium2-(2-amino-5-bromophenyl)-2-oxoacetate 95+%
5g
$ 1732.00

Crysdot
Potassium2-(2-amino-5-bromophenyl)-2-oxoacetate 95+%
1g
$ 495.00

American Custom Chemicals Corporation
POTASSIUM-2-(2-AMINO-5-BROMOPHENYL)-2-OXOACETATE 95.00%
5MG
$ 496.89

Alichem
Potassium2-(2-amino-5-bromophenyl)-2-oxoacetate
5g
$ 1749.32

Alichem
Potassium2-(2-amino-5-bromophenyl)-2-oxoacetate
1g
$ 544.50

Total 2 raw suppliers

Chemical Property of 2-(2-aMino-5-broMophenyl)-2-oxoacetic acid

Chemical Property:

PSA：83.22000
LogP:0.54510
Storage Temp.:Keep in dark place,Inert atmosphere,Room temperature

Purity/Quality:

97% ^*data from raw suppliers

Potassium2-(2-amino-5-bromophenyl)-2-oxoacetate 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 2-(2-aMino-5-broMophenyl)-2-oxoacetic acid

There total 2 articles about 2-(2-aMino-5-broMophenyl)-2-oxoacetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 87-48-9
5-Bromo-1H-indole-2,3-dione

: 120095-19-4
5-Bromoisatic acid potassium salt

Guidance literature:: With alkaline solution;

Reference yield:

: 91-56-5,1186480-61-4,84788-92-1
indole-2,3-dione

: 120095-19-4
5-Bromoisatic acid potassium salt

Guidance literature:: Multi-step reaction with 2 steps

1: acetic acid; bromine / 8 h / Reflux

2: potassium carbonate; water / ethanol / Inert atmosphere; Reflux

With water; bromine; potassium carbonate; acetic acid; In ethanol;
DOI:10.1002/cmdc.201600266

Reference yield:

: 120095-19-4
5-Bromoisatic acid potassium salt

: 130471-56-6
{5-Bromo-2-[2-oxo-1-(triphenyl-λ⁵-phosphanylidene)-propylazo]-phenyl}-oxo-acetic acid methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) 20percent aq. H₂SO₄, NaNO₂ 2) NaOAc / 1) water, 0 deg C 2) MeOH, 0 deg C, 1h

2: HCl / 2 h / Heating

3: 77 percent / Et₃N / acetonitrile / Ambient temperature

With hydrogenchloride; sulfuric acid; sodium acetate; triethylamine; sodium nitrite; In acetonitrile;