1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE

Base Information

Chemical Name:1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE
CAS No.:102090-24-4
Molecular Formula:C₁₇H₂₁NO₃
Molecular Weight:287.359
Hs Code.:
Mol file:102090-24-4.mol

Synonyms:1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE;N-Boc-2-hydroxy-2-(1-naphthalenyl)ethylaMine;tert-butyl 2-hydroxy-2-(naphthalen-1-yl)ethylcarbamate

Suppliers and Price of 1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Acrotein
N-Boc-2-hydroxy-2-(1-naphthalenyl)ethylamine 97%
0.5g
$ 220.00

Total 3 raw suppliers

Chemical Property of 1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE

Chemical Property:

PSA：58.56000
LogP:3.78880

Purity/Quality:

99.90% ^*data from raw suppliers

N-Boc-2-hydroxy-2-(1-naphthalenyl)ethylamine 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE

There total 3 articles about 1,1-DIMETHYLETHYL [2-HYDROXY-2-(1-NAPHTHALENYL)ETHYL]CARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 23913-55-5
β-Hydroxy-β-(1-naphthyl)ethylamine

: 24424-99-5
di-tert-butyl dicarbonate

: 102090-24-4
1,1-dimethylethyl [2-hydroxy-2-(1-naphthalenyl)ethyl]carbamate

Guidance literature:: In dichloromethane; at 20 ℃; for 12h;

Reference yield:

: 66-77-3
1-naphthaldehyde

: 102090-24-4
1,1-dimethylethyl [2-hydroxy-2-(1-naphthalenyl)ethyl]carbamate

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid / diethyl ether / 20 h / 0 - 25 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

3: dichloromethane / 12 h / 20 °C

With lithium aluminium tetrahydride; acetic acid; In tetrahydrofuran; diethyl ether; dichloromethane;

Reference yield:

: 121950-19-4,136983-94-3,143954-79-4,97798-35-1
1-naphthyl cyanohydrin

: 102090-24-4
1,1-dimethylethyl [2-hydroxy-2-(1-naphthalenyl)ethyl]carbamate

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 2 h / 0 °C

2: dichloromethane / 12 h / 20 °C

With lithium aluminium tetrahydride; In tetrahydrofuran; dichloromethane;