6,7,14,15,22,23-hexaoxatrispiro[4.2.5~8~.2.5~16~.2~5~]tricosane

Base Information

Chemical Name:6,7,14,15,22,23-hexaoxatrispiro[4.2.5~8~.2.5~16~.2~5~]tricosane
CAS No.:6789-46-4
Molecular Formula:C17H28O6
Molecular Weight:328.406
Hs Code.:

Synonyms:

Suppliers and Price of 6,7,14,15,22,23-hexaoxatrispiro[4.2.5~8~.2.5~16~.2~5~]tricosane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 4 raw suppliers

Chemical Property of 6,7,14,15,22,23-hexaoxatrispiro[4.2.5~8~.2.5~16~.2~5~]tricosane

Chemical Property:

Vapor Pressure:2.7E-06mmHg at 25°C
Boiling Point:401.6°Cat760mmHg
Flash Point:160.2°C
Density:1.2g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6,7,14,15,22,23-hexaoxatrispiro[4.2.5~8~.2.5~16~.2~5~]tricosane

There total 4 articles about 6,7,14,15,22,23-hexaoxatrispiro[4.2.5~8~.2.5~16~.2~5~]tricosane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 2699-12-9
bis-(1-hydroperoxycyclohexyl)peroxide

: 931-94-2
1,1-dimethoxycyclopentane

: 6789-46-4
6,7,14,15,22,23-hexaoxatrispiro[4.2.5⁸.2.5¹⁶.2⁵]tricosane

Guidance literature:: With boron trifluoride diethyl etherate; In diethyl ether; at 20 - 25 ℃; for 4h;
DOI:10.1021/jo071072c

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 6789-46-4
6,7,14,15,22,23-hexaoxatrispiro[4.2.5⁸.2.5¹⁶.2⁵]tricosane

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / aq. H₂O₂; H₂SO₄ / 1 h / 10 - 15 °C

2: 82 percent / BF₃*Et₂O / diethyl ether / 4 h / 20 - 25 °C

With sulfuric acid; boron trifluoride diethyl etherate; dihydrogen peroxide; In diethyl ether;
DOI:10.1021/jo071072c

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 6789-46-4
6,7,14,15,22,23-hexaoxatrispiro[4.2.5⁸.2.5¹⁶.2⁵]tricosane

Guidance literature:: Multi-step reaction with 2 steps

1: dihydrogen peroxide; sulfuric acid / water / 1 h

2: boron trifluoride diethyl etherate / diethyl ether / 16 h / 0 - 20 °C

With sulfuric acid; boron trifluoride diethyl etherate; dihydrogen peroxide; In diethyl ether; water;
DOI:10.1021/acs.joc.1c00663