CHEMBRDG-BB 4010333

Base Information

• Chemical Name: CHEMBRDG-BB 4010333
• CAS No.: 60759-10-6
• Molecular Formula: C9H8N2S
• Molecular Weight: 176.242
• Hs Code.: 2934100090
• Mol file: 60759-10-6.mol

Synonyms:CHEMBRDG-BB 4010333;4-(1,3-THIAZOL-4-YL)ANILINE;4-(1,3-thiazol-4-yl)aniline(SALTDATA: FREE)

Chemical Property of CHEMBRDG-BB 4010333

Chemical Property:

• Vapor Pressure: 0mmHg at 25°C
• Melting Point: 99 °C
• Boiling Point: 347.414°C at 760 mmHg
• PKA: 3.24±0.10(Predicted)
• Flash Point: 163.91°C
• PSA: 67.15000
• Density: 1.262g/cm³
• LogP: 2.97350

Purity/Quality:

98%+ ^*data from raw suppliers

4-(4-Aminophenyl)thiazole ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi
• Statements: 41
• Safety Statements: 26-39

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of CHEMBRDG-BB 4010333

There total 8 articles about CHEMBRDG-BB 4010333 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-(4-nitro-phenyl)-thiazole (3704-42-5) → 4-(4-aminophenyl)thiazole (60759-10-6)

Guidance literature:

With methanol; palladium on activated charcoal; Hydrogenation;

Reference yield:

ethyl 4-(4-nitrophenyl)-1,3-thiazole-2-carboxylate (53101-04-5) → 4-(4-amino-phenyl)-thiazole-2-carboxylic acid ethyl ester (491577-82-3) + 4-(4-aminophenyl)thiazole (60759-10-6)

Guidance literature:

ethyl 4-(4-nitrophenyl)-1,3-thiazole-2-carboxylate; With hydrogenchloride; tin(II) chloride dihdyrate; In ethanol; water; for 2h; Reflux;

With potassium hydroxide; In ethanol; water; at 0 ℃;

Reference yield:

4-Nitrophenacyl bromide (99-81-0) → 4-(4-aminophenyl)thiazole (60759-10-6)

Guidance literature:

Multi-step reaction with 2 steps

1.1: diphosphorus pentasulfide / 1,3-dioxane / 1 h / Reflux; Inert atmosphere

1.2: 1 h / Reflux

2.1: ammonium chloride / iron / ethanol / 2 h / Reflux

With diphosphorus pentasulfide; ammonium chloride; iron; In 1,3-dioxane; ethanol;

upstream raw materials:

4-(4-nitro-phenyl)-thiazole

thiocarboxamide

4-aminophenacyl chloride

1-chloroacetophenone

Downstream raw materials:

1,3-bis-(4-thiazol-4-yl-phenyl)-thiourea

1-(4-isopropoxy-phenyl)-3-(4-thiazol-4-yl-phenyl)-thiourea

N-{4-[bis-(2-chloro-ethyl)-amino]-benzylidene}-4-thiazol-4-yl-aniline

1-(4-methoxy-phenyl)-3-(4-thiazol-4-yl-phenyl)-thiourea

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