2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane

Base Information

Chemical Name:2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane
CAS No.:552845-84-8
Molecular Formula:C11H13BrO4
Molecular Weight:289.126
Hs Code.:2932999099
DSSTox Substance ID:DTXSID30583038
Wikidata:Q82474549
Mol file:552845-84-8.mol

Synonyms:552845-84-8;2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane;1-bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene;2-(5-BROMO-2,4-DIMETHOXY-PHENYL)-[1,3]DIOXOLANE;MFCD06209473;C11H13BrO4;SCHEMBL6040717;DTXSID30583038;WGGFSFMCMNCRPP-UHFFFAOYSA-N;CXA84584;AKOS016023234;SB37636;AS-47201;CS-0341928;F12604

Suppliers and Price of 2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Rieke Metals
1-bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene 97%
1g
$ 318.00

Rieke Metals
1-bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene 97%
2g
$ 515.00

Rieke Metals
1-bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene 97%
5g
$ 846.00

Matrix Scientific
1-Bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene
1g
$ 319.00

Matrix Scientific
1-Bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene
5g
$ 753.00

Matrix Scientific
1-Bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene
2g
$ 489.00

J&W Pharmlab
2-(5-Bromo-2,4-dimethoxy-phenyl)-[1,3]dioxolane 96%
50mg
$ 125.00

Crysdot
2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane 95+%
5g
$ 746.00

Chemenu
1-Bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene 95%
5g
$ 704.00

American Custom Chemicals Corporation
1-BROMO-2,4-DIMETHOXY-5-(1,3-DIOXOLAN-2-YL)BENZENE 95.00%
1G
$ 958.07

Total 10 raw suppliers

Chemical Property of 2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane

Chemical Property:

Vapor Pressure:0mmHg at 25°C
Boiling Point:353.108°C at 760 mmHg
Flash Point:144.036°C
PSA：36.92000
Density:1.452g/cm³
LogP:2.51170
XLogP3:2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:3
Exact Mass:287.99972
Heavy Atom Count:16
Complexity:220

Purity/Quality:

97% ^*data from raw suppliers

1-bromo-2,4-dimethoxy-5-(1,3-dioxolan-2-yl)benzene 97% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:COC1=CC(=C(C=C1C2OCCO2)Br)OC

Technology Process of 2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane

There total 2 articles about 2-(5-Bromo-2,4-dimethoxyphenyl)-1,3-dioxolane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

: 130333-46-9
5-bromo-2, 4-dimethoxybenzaldehyde

: 107-21-1
ethylene glycol

: 552845-84-8
2-(5-bromo-2,4-dimethoxy-phenyl)-[1,3]dioxolane

Guidance literature:: toluene-4-sulfonic acid; In benzene; for 6h; Heating;
DOI:10.1021/jm0614230

Reference yield:

: 613-45-6
2,4-Dimethoxybenzaldehyde

: 552845-84-8
2-(5-bromo-2,4-dimethoxy-phenyl)-[1,3]dioxolane

Guidance literature:: Multi-step reaction with 2 steps

1: bromine; acetic acid / 2 h / 70 °C

2: toluene-4-sulfonic acid / benzene / Dean-Stark; Reflux

With bromine; toluene-4-sulfonic acid; acetic acid; In benzene;
DOI:10.1021/jo401756q