BENZYL 4-BROMOPHENETHYLCARBAMATE

Base Information

• Chemical Name: BENZYL 4-BROMOPHENETHYLCARBAMATE
• CAS No.: 191170-76-0
• Molecular Formula: C16H16BrNO2
• Molecular Weight: 334.213
• Mol file: 191170-76-0.mol

Synonyms:BENZYL 4-BROMOPHENETHYLCARBAMATE

Chemical Property of BENZYL 4-BROMOPHENETHYLCARBAMATE

Chemical Property:

• Boiling Point: 473.7±38.0 °C(Predicted)
• PKA: 12.38±0.46(Predicted)
• PSA: 38.33000
• Density: 1.367±0.06 g/cm3(Predicted)
• LogP: 4.30890
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

99% ^*data from raw suppliers

Benzyl4-bromophenethylcarbamate ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of BENZYL 4-BROMOPHENETHYLCARBAMATE

There total 5 articles about BENZYL 4-BROMOPHENETHYLCARBAMATE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

4-Bromophenethylamine (73918-56-6) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl N-[2-(4-bromophenyl)ethyl]carbamate (191170-76-0)

Guidance literature:

With sodium hydrogencarbonate; In water; at 20 ℃; for 1h;

Reference yield: 100.0%

2-(4-bromophenyl)-1-aminoethane hydrochloride (39260-89-4) + benzyl chloroformate (501-53-1,94274-21-2) → benzyl N-[2-(4-bromophenyl)ethyl]carbamate (191170-76-0)

Guidance literature:

With sodium carbonate; In tetrahydrofuran; water; at 0 - 20 ℃; for 2h;

Reference yield: 71.0%

4-bromophenethanol (4654-39-1) + N-[[[(benzyloxy)carbonyl]azanide]sulfonyl]-N,N-diethylethylammonium (439585-11-2) → benzyl N-[2-(4-bromophenyl)ethyl]carbamate (191170-76-0)

Guidance literature:

In benzene; at 50 - 85 ℃;

DOI:10.1016/S0040-4039(02)00659-7

upstream raw materials:

4-bromophenethanol

N-[[[(benzyloxy)carbonyl]azanide]sulfonyl]-N,N-diethylethylammonium

benzyl alcohol

4-Bromophenethylamine

Downstream raw materials:

C₂₇H₂₉NO₄

C₂₈H₃₁NO₅

Refernces

• 1、 -. "THIENOPYRIDINE CARBOXAMIDES AS UBIQUITIN-SPECIFIC PROTEASE INHIBITORS". Paragraph 00391. . Retrieved 2017/09/05.
• 2、 -. "INHIBITION OF BACTERIAL BIOFILMS WITH ARYL CARBAMATES". Page/Page column 33. . Retrieved 2012/02/01.