N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiiMide

Base Information

• Chemical Name: N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiiMide
• CAS No.: 245049-70-1
• Molecular Formula: C8H6N2O6
• Molecular Weight: 226.145
• Mol file: 245049-70-1.mol

Synonyms:N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiiMide;N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiimide

Chemical Property of N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiiMide

Chemical Property:

• Boiling Point: 547.6±60.0 °C(Predicted)
• PKA: 7.18±0.20(Predicted)
• PSA: 115.22000
• Density: 2.227±0.06 g/cm3(Predicted)
• LogP: -2.14340

Purity/Quality:

98% ^*data from raw suppliers

N,N''-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiimide ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiiMide

There total 1 articles about N,N'-Dihydroxy-1,2,3,4-cyclobutanetetracarboxdiiMide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

cyclobutanetetracarboxylic dianhydride (4415-87-6) → N,N'-dihydroxycyclobutanetetracarboxylic diimide (245049-70-1)

Guidance literature:

With pyridine; hydroxylamine hydrochloride; at 20 - 90 ℃; for 0.25h;

Reference yield: 58.4%

N,N'-dihydroxycyclobutanetetracarboxylic diimide (245049-70-1) + 3-(Trifluoromethyl)benzenesulfonyl chloride (777-44-6) → tetrahydro-2,5-bis(3-trifluoromethylphenylsulfonyloxy)cyclobuta[1,2-c:3,4-c']dipyrrole-1,3,4,6(2H,5H)-tetrone (535952-25-1)

Guidance literature:

With pyridine; In N,N-dimethyl acetamide; at 20 ℃; for 1h;

upstream raw materials:

cyclobutanetetracarboxylic dianhydride

Downstream raw materials:

tetrahydro-2,5-bis(3-trifluoromethylphenylsulfonyloxy)cyclobuta[1,2-c:3,4-c']dipyrrole-1,3,4,6(2H,5H)-tetrone