Ethanone, 1-(2-thiazolyl)-, oxime (9CI)

Base Information

• Chemical Name: Ethanone, 1-(2-thiazolyl)-, oxime (9CI)
• CAS No.: 98025-45-7
• Molecular Formula: C5H6N2OS
• Molecular Weight: 142.17894
• Hs Code.: 2934100090
• Mol file: 98025-45-7.mol

Synonyms:Ethanone, 1-(2-thiazolyl)-, oxime (9CI);Ethanone, 1-(2-thiazolyl)-, oxiMe

Chemical Property of Ethanone, 1-(2-thiazolyl)-, oxime (9CI)

Chemical Property:

• PSA: 73.72000
• LogP: 1.34130

Purity/Quality:

1-(1,3-THIAZOL-2-YL)-1-ETHANONE OXIME 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Ethanone, 1-(2-thiazolyl)-, oxime (9CI)

There total 3 articles about Ethanone, 1-(2-thiazolyl)-, oxime (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

2-Acetylthiazole (24295-03-2,260998-74-1) → 2-[1-(hydroxyimino)ethyl]-thiazole (98025-45-7)

Guidance literature:

With hydroxylamine hydrochloride; triethylamine; In ethanol; at 120 ℃; for 0.333333h; Microwave irradiation;

DOI:10.1016/j.bmc.2009.03.041

Reference yield:

3-thiazol-2-yl-acrylic acid (52396-77-7) → 2-[1-(hydroxyimino)ethyl]-thiazole (98025-45-7) + 3-amino-3-thiazol-2-yl-propionic acid (52396-78-8)

Guidance literature:

With ethanol; hydroxylamine;

Reference yield:

2-(2-methyl-1,3-dioxolan-2-yl)-1,3-thiazole (24295-06-5) → 2-[1-(hydroxyimino)ethyl]-thiazole (98025-45-7)

Guidance literature:

Multistep reaction; (i) aq. HBr, (ii) NH₂OH;

DOI:10.1039/j39690002270

upstream raw materials:

3-thiazol-2-yl-acrylic acid

2-(2-methyl-1,3-dioxolan-2-yl)-1,3-thiazole

2-Acetylthiazole

Downstream raw materials:

1-(thiazol-2-yl)ethan-1-amine

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