1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester

Base Information

Chemical Name:1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester
CAS No.:1596367-55-3
Molecular Formula:C14H20BNO3
Molecular Weight:261.129
Hs Code.:
Mol file:1596367-55-3.mol

Synonyms:1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester

Suppliers and Price of 1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 10 raw suppliers

Chemical Property of 1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester

Chemical Property:

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

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Technology Process of 1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester

There total 4 articles about 1-Cyclopropyl-6-oxo-1,6-dihydropyridine-3-boronic acid pinacol ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1193334-67-6
5-bromo-1-cyclopropyl-1,2-dihydropyridin-2-one

: 73183-34-3
bis(pinacol)diborane

: 1596367-55-3
1-cyclopropyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2-dihydropyridin-2-one

Guidance literature:: With 1,1'-bis-(diphenylphosphino)ferrocene; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; In 1,4-dioxane; at 90 ℃; for 4h; Inert atmosphere;

Reference yield: 36.43%

: 1596367-55-3
1-cyclopropyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2-dihydropyridin-2-one

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium acetate; In dimethyl sulfoxide; at 90 ℃; for 4h; Inert atmosphere;

Reference yield:

: 13466-38-1,49843-23-4
5-bromopyridin-2(1H)-one

: 1596367-55-3
1-cyclopropyl-5-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)-1,2-dihydropyridin-2-one

Guidance literature:: Multi-step reaction with 2 steps

1: sodium carbonate; copper diacetate; 4,4'-di-tert-butyl-2,2'-bipyridine / 1,2-dichloro-ethane / 12 h / 70 °C / Inert atmosphere

2: potassium acetate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂ / tetrahydrofuran / 2 h / 80 °C / Inert atmosphere

With dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate; copper diacetate; sodium carbonate; 4,4'-di-tert-butyl-2,2'-bipyridine; In tetrahydrofuran; 1,2-dichloro-ethane;