2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester

Base Information

Chemical Name:2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester
CAS No.:75422-05-8
Molecular Formula:C18H18O7
Molecular Weight:0
Hs Code.:
Mol file:75422-05-8.mol

Synonyms:2,4-Dihydroxy-3,6-dimethylbenzoic acid 3-hydroxy-4-(methoxycarbonyl)-5-methylphenyl ester;2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester

Suppliers and Price of 2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester

Chemical Property:

Melting Point:142 °C
PSA：113.29000
LogP:2.73440

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester

There total 5 articles about 2-Hydroxy-4-[(2,4-dihydroxy-3,6-dimethylbenzoyl)oxy]-6-methylbenzoic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 4-Benzyloxy-2-hydroxy-3,6-dimethyl-benzoic acid 3-hydroxy-4-methoxycarbonyl-5-methyl-phenyl ester

: 75422-05-8
4-(2,4-dihydroxy-3,6-dimethyl-benzoyloxy)-2-hydroxy-6-methyl-benzoic acid methyl ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In ethyl acetate;
DOI:10.1016/S0223-5234(00)00132-X

Reference yield:

: 3187-58-4
methyl orsellinate

: 75422-05-8
4-(2,4-dihydroxy-3,6-dimethyl-benzoyloxy)-2-hydroxy-6-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / (CF₃CO)2O / toluene / 20 °C

2: 87 percent / H₂ / 10 percent Pd/C / ethyl acetate

With hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethyl acetate; toluene; 1: Condensation / 2: Hydrogenolysis;
DOI:10.1016/S0223-5234(00)00132-X

Reference yield:

: 56410-32-3
4-benzyloxy-2-hydroxy-3,6-dimethylbenzoic acid

: 75422-05-8
4-(2,4-dihydroxy-3,6-dimethyl-benzoyloxy)-2-hydroxy-6-methyl-benzoic acid methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 49 percent / (CF₃CO)2O / toluene / 20 °C

2: 87 percent / H₂ / 10 percent Pd/C / ethyl acetate

With hydrogen; trifluoroacetic anhydride; palladium on activated charcoal; In ethyl acetate; toluene; 1: Condensation / 2: Hydrogenolysis;
DOI:10.1016/S0223-5234(00)00132-X