6,10,10-trimethyl-2-methylidene-5-nitro-6-nitrosobicyclo[7.2.0]undecane

Base Information

• Chemical Name: 6,10,10-trimethyl-2-methylidene-5-nitro-6-nitrosobicyclo[7.2.0]undecane
• CAS No.: 28834-17-5
• Molecular Formula: C₁₅H₂₄N₂O₃
• Molecular Weight: 280.367
• Mol file: 28834-17-5.mol

Synonyms:Bicyclo[7.2.0]undecane,6,10,10-trimethyl-2-methylene-5-nitro-6-nitroso-, [1S-(1a,5a,6b,9b)]-; Caryophyllene nitrosite

Chemical Property of 6,10,10-trimethyl-2-methylidene-5-nitro-6-nitrosobicyclo[7.2.0]undecane

Chemical Property:

• Vapor Pressure: 1.26E-05mmHg at 25°C
• Boiling Point: 368.6°Cat760mmHg
• Flash Point: 176.7°C
• Density: 1.21g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 6,10,10-trimethyl-2-methylidene-5-nitro-6-nitrosobicyclo[7.2.0]undecane

There total 3 articles about 6,10,10-trimethyl-2-methylidene-5-nitro-6-nitrosobicyclo[7.2.0]undecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(E)-β-caryophyllene (17627-40-6) → caryophyllene nitrosite (28834-17-5) + dinitrocaryophyllene (100362-04-7)

Guidance literature:

With acetic acid; sodium nitrite; In Petroleum ether; dark, 1.) 10 deg C, 15 min; 2.) 0 deg C, 30 min;

DOI:10.1039/P29850000971

Reference yield:

β-caryophyllene (87-44-5) → Caryophyllinnitrosit (28834-17-5)

Guidance literature:

With acetic acid; Petroleum ether; sodium nitrite;

Reference yield:

→ Caryophyllinnitrosit (28834-17-5)

Guidance literature:

Caryophyllin u. NaNO2;

upstream raw materials:

β-caryophyllene

(E)-β-caryophyllene