1-(4-methoxybenzyl)-5-methyl-6,7-dihydro-1H-indazol-4(5H)-one

Base Information

Chemical Name:1-(4-methoxybenzyl)-5-methyl-6,7-dihydro-1H-indazol-4(5H)-one
CAS No.:1355249-10-3
Molecular Formula:C₁₆H₁₈N₂O₂
Molecular Weight:0
Hs Code.:
Mol file:1355249-10-3.mol

Synonyms:1-(4-methoxybenzyl)-5-methyl-6,7-dihydro-1H-indazol-4(5H)-one

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Chemical Property of 1-(4-methoxybenzyl)-5-methyl-6,7-dihydro-1H-indazol-4(5H)-one

Chemical Property:

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Technology Process of 1-(4-methoxybenzyl)-5-methyl-6,7-dihydro-1H-indazol-4(5H)-one

There total 2 articles about 1-(4-methoxybenzyl)-5-methyl-6,7-dihydro-1H-indazol-4(5H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1355249-05-6
C₁₅H₁₈N₂O₄S

: 824-94-2
p-methoxybenzyl chloride

: 1355249-11-4
C₁₆H₁₈N₂O₂

: 1355249-10-3
C₁₆H₁₈N₂O₂

: 1355249-08-9
C₁₆H₁₈N₂O₂

: 1355249-09-0
C₁₆H₁₈N₂O₂

Guidance literature:: C₁₅H₁₈N₂O₄S; With hydrogenchloride; In water; butan-1-ol; at 110 ℃; for 1h;

p-methoxybenzyl chloride; With potassium carbonate; In acetonitrile; for 3h; Reflux;

Reference yield:

: 14203-46-4
4-methyl-cyclohexane-1,3-dione

: 1355249-11-4
C₁₆H₁₈N₂O₂

: 1355249-10-3
C₁₆H₁₈N₂O₂

: 1355249-08-9
C₁₆H₁₈N₂O₂

: 1355249-09-0
C₁₆H₁₈N₂O₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: dichloromethane / 1 h / 20 °C

2.1: methanol / 0.5 h / 20 °C

3.1: hydrogenchloride / butan-1-ol; water / 1 h / 110 °C

3.2: 3 h / Reflux

With hydrogenchloride; In methanol; dichloromethane; water; butan-1-ol;