6-Bromobenzo[d]isoxazol-3(2H)-one

Base Information

Chemical Name:6-Bromobenzo[d]isoxazol-3(2H)-one
CAS No.:65685-51-0
Molecular Formula:C7H4BrNO2
Molecular Weight:214.018
Hs Code.:2934999090
European Community (EC) Number:946-562-9
DSSTox Substance ID:DTXSID20459435
Wikidata:Q82283201
Mol file:65685-51-0.mol

Synonyms:65685-51-0;6-Bromobenzo[d]isoxazol-3(2H)-one;6-bromo-1,2-benzisoxazol-3-ol;6-bromobenzo[d]isoxazol-3-ol;6-bromo-1,2-benzoxazol-3-one;6-bromo-1,2-benzoxazol-3-ol;SCHEMBL3526289;AMY5097;DTXSID20459435;ZXDOSRLQEYIVJC-UHFFFAOYSA-N;MFCD09842495;MFCD13193078;AKOS005073324;LD-0722;6-Bromo-1,2-benzisoxazol-3 (2H)-one;SY112425;CS-0085269;FT-0681323;EN300-200296;J-518421

Suppliers and Price of 6-Bromobenzo[d]isoxazol-3(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

TRC
6-Bromo-1,2-benzisoxazol-3-ol
50mg
$ 175.00

Matrix Scientific
6-Bromo-1,2-benzisoxazol-3-ol > 90
1g
$ 756.00

Matrix Scientific
6-Bromo-1,2-benzisoxazol-3-ol > 90
500mg
$ 599.00

Crysdot
6-Bromobenzo[d]isoxazol-3(2H)-one 97%
10g
$ 1664.00

Crysdot
6-Bromobenzo[d]isoxazol-3(2H)-one 97%
5g
$ 976.00

Crysdot
6-Bromobenzo[d]isoxazol-3(2H)-one 97%
1g
$ 301.00

Chemenu
6-bromobenzo[d]isoxazol-3(2H)-one 96%
1g
$ 298.00

Chemenu
6-bromobenzo[d]isoxazol-3(2H)-one 96%
5g
$ 966.00

Chemenu
6-bromobenzo[d]isoxazol-3(2H)-one 96%
100mg
$ 58.00

American Custom Chemicals Corporation
6-BROMOBENZO[D]ISOXAZOL-3-(2H)-ONE 95.00%
1G
$ 1270.50

Total 17 raw suppliers

Chemical Property of 6-Bromobenzo[d]isoxazol-3(2H)-one

Chemical Property:

Melting Point:219-221°
PKA:13.36±0.20(Predicted)
PSA：46.00000
Density:1.809±0.06 g/cm3(Predicted)
LogP:1.88360
Storage Temp.:2-8°C
XLogP3:1.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:212.94254
Heavy Atom Count:11
Complexity:185

Purity/Quality:

97% ^*data from raw suppliers

6-Bromo-1,2-benzisoxazol-3-ol ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC2=C(C=C1Br)ONC2=O

Technology Process of 6-Bromobenzo[d]isoxazol-3(2H)-one

There total 6 articles about 6-Bromobenzo[d]isoxazol-3(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 61799-79-9
4-bromo-2-hydroxy-benzenecarbohydroxamic acid

: 65685-51-0
6-bromo-1,2-benzoxazol-3-ol

Guidance literature:: With 1,1'-carbonyldiimidazole; In tetrahydrofuran; for 2h; Reflux;

Reference yield: 31.0%

: 546-88-3
acetylhydroxamic acid

: 179232-29-2
methyl 4-bromo-2-fluorobenzoate

: 65685-51-0
6-bromo-1,2-benzoxazol-3-ol

Guidance literature:: acetylhydroxamic acid; With potassium tert-butylate; In N,N-dimethyl-formamide; for 0.5h;

methyl 4-bromo-2-fluorobenzoate; In N,N-dimethyl-formamide; at 20 ℃; for 240h;

Reference yield:

: 1666-28-0
4-bromosalicylic acid

: 65685-51-0
6-bromo-1,2-benzoxazol-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / 12 h / 75 °C

2: hydroxylamine hydrochloride; sodium hydroxide / water; 1,4-dioxane / 18 h / 20 °C

3: 1,1'-carbonyldiimidazole / tetrahydrofuran / 2 h / Reflux

With sulfuric acid; hydroxylamine hydrochloride; 1,1'-carbonyldiimidazole; sodium hydroxide; In tetrahydrofuran; 1,4-dioxane; water;