1-(4-Chlorophenyl)-1-phenylhydrazine

Base Information

• Chemical Name: 1-(4-Chlorophenyl)-1-phenylhydrazine
• CAS No.: 58263-75-5
• Molecular Formula: C12H11ClN2
• Molecular Weight: 218.68

Synonyms:1-(4-Chlorophenyl)-1-phenylhydrazine

Chemical Property of 1-(4-Chlorophenyl)-1-phenylhydrazine

Chemical Property:

• PSA: 29.26000
• LogP: 4.05210

Purity/Quality:

99% ^*data from raw suppliers

1-(4-Chlorophenyl)-1-phenylhydrazine 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 1-(4-Chlorophenyl)-1-phenylhydrazine

There total 5 articles about 1-(4-Chlorophenyl)-1-phenylhydrazine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

N-(N-4-chlorophenyl-N-phenylamino)phthalimide (262606-99-5) → N-(4-chloro-phenyl)-N-phenyl-hydrazine (58263-75-5)

Guidance literature:

With hydrazine hydrate; In ethanol; for 6h; Heating;

DOI:10.1080/00397910008087300

Reference yield:

N-(N-4-chlorophenylamino)phthalimide (107940-74-9) → N-(4-chloro-phenyl)-N-phenyl-hydrazine (58263-75-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / Cu(OAc)2; Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 70 percent / NH₂NH₂*H₂O / ethanol / 6 h / Heating

With copper diacetate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; 1: Phenylation / 2: trans-amination;

DOI:10.1080/00397910008087300

Reference yield:

triphenylbismuthane (603-33-8) → N-(4-chloro-phenyl)-N-phenyl-hydrazine (58263-75-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 98 percent / Cu(OAc)2; Et₃N / CH₂Cl₂ / 24 h / 20 °C

2: 70 percent / NH₂NH₂*H₂O / ethanol / 6 h / Heating

With copper diacetate; hydrazine hydrate; triethylamine; In ethanol; dichloromethane; 1: Phenylation / 2: trans-amination;

DOI:10.1080/00397910008087300

upstream raw materials:

(4-chloro-phenyl)-nitroso-phenyl-amine

N-(N-4-chlorophenyl-N-phenylamino)phthalimide

N-(N-4-chlorophenylamino)phthalimide

triphenylbismuthane

Downstream raw materials:

N'-(4-chloro-phenyl)-N'-phenyl-N-picryl-hydrazine

N-(4-chloro-phenyl)-N-phenyl-N'-picryl-hydrazine

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