Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-galactopyranoside

Base Information

• Chemical Name: Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-galactopyranoside
• CAS No.: 10049-88-4
• Molecular Formula: C12H23NO6
• Molecular Weight: 277.318
• Mol file: 10049-88-4.mol

Synonyms:Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-galactopyranoside

Chemical Property of Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-galactopyranoside

Chemical Property:

• Boiling Point: None °C
• PSA: 75.25000
• LogP: -0.07030

Purity/Quality:

98%,99%, ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-galactopyranoside

There total 8 articles about Methyl 2-(acetylamino)-3-O,4-O,6-O-trimethyl-2-deoxy-α-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C77H130N2O26 (116237-66-2) → methyl 2-hydroxy-3,4,6-tri-O-methyl-α-D-glucopyranoside (13479-66-8) + Methyl α-sophorosid-per-O-methyl (71606-24-1) + methyl 2,3,4,6-tetra-O-methyl-α-D-glucopyranoside (605-81-2) + methyl-(2-acetylamino-tri-O-methyl-2-deoxy-α-D-galactopyranoside) (10049-88-4)

Guidance literature:

With hydrogenchloride; In methanol; at 70 ℃; for 3h; Further byproducts given;

DOI:10.1021/jo00260a025

Reference yield:

methyl-(2-acetylamino-tri-O-methyl-2-deoxy-β-D-galactopyranoside) (7437-12-9) → methyl-(2-acetylamino-tri-O-methyl-2-deoxy-α-D-galactopyranoside) (10049-88-4)

Guidance literature:

With hydrogenchloride; methanol;

DOI:10.1039/jr9440000272

Reference yield:

methyl-[O3,O4,O6-trimethyl-O2-(toluene-4-sulfonyl)-β-D-galactopyranoside] (36480-32-7) → methyl-(2-acetylamino-O3,O4,O6-trimethyl-2-deoxy-β-D-talopyranoside) (6195-86-4,7323-01-5,7380-60-1,7384-32-9,7437-12-9,7437-13-0,10049-88-4,42756-56-9,96744-17-1,110715-58-7)

Guidance literature:

With methanol; ammonia; Behandeln des Reaktionsprodukts in Methanol mit Acetanhydrid;

DOI:10.1039/jr9440000522

upstream raw materials:

methyl-[O³,O⁴,O⁶-trimethyl-O²-(toluene-4-sulfonyl)-β-D-galactopyranoside]

methanol

ammonia

methyl-(2-acetylamino-tri-O-methyl-2-deoxy-β-D-galactopyranoside)

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