Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI)

Base Information

Chemical Name:Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI)
CAS No.:170030-61-2
Molecular Formula:C11H16N2O2
Molecular Weight:208.26
Hs Code.:
Mol file:170030-61-2.mol

Synonyms:Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI)

Suppliers and Price of Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI)

Chemical Property:

PSA：78.34000
LogP:2.96870

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI)

There total 2 articles about Benzoic acid, 3,5-diamino-, 1,1-dimethylethyl ester (9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 5342-97-2
t-butyl 3,5-dinitrobenzoate

: 170030-61-2
tert-butyl 3,5-diaminobenzoate

Guidance literature:: With iron; ammonium chloride; In ethanol; water; at 95 ℃;
DOI:10.1002/chem.202003524

Reference yield:

: 99-34-3
3,5-dinitrobenzoic acid

: 170030-61-2
tert-butyl 3,5-diaminobenzoate

Guidance literature:: Multi-step reaction with 3 steps

1: phosgene / dichloromethane; N,N-dimethyl-formamide / 2 h / Inert atmosphere

2: tetrahydrofuran / 5 h / 20 °C / Inert atmosphere

3: 10% Pd/C; hydrogen / methanol / 20 °C / Inert atmosphere

With phosgene; 10% Pd/C; hydrogen; In tetrahydrofuran; methanol; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc35004a

Reference yield: 82.0%

: 170030-61-2
tert-butyl 3,5-diaminobenzoate

: 105-36-2
ethyl bromoacetate

: tetraethyl 2,2',2'',2'''-((5-(tert-butoxycarbonyl)-1,3-phenylene)bis(azanetriyl))tetraacetate

Guidance literature:: With N-ethyl-N,N-diisopropylamine; sodium iodide; In acetonitrile; for 120h; Reflux; Inert atmosphere;
DOI:10.1002/chem.202003524