3-BROMOPHENYL CYCLOPROPYL KETONE

Base Information

• Chemical Name: 3-BROMOPHENYL CYCLOPROPYL KETONE
• CAS No.: 693774-26-4
• Molecular Formula: C10H9BrO
• Molecular Weight: 225.085
• Hs Code.: 2914700090
• Mol file: 693774-26-4.mol

Synonyms:3-BROMOPHENYL CYCLOPROPYL KETONE

Chemical Property of 3-BROMOPHENYL CYCLOPROPYL KETONE

Chemical Property:

• Vapor Pressure: 0.000952mmHg at 25°C
• Boiling Point: 303.1°C at 760 mmHg
• Flash Point: 97.2°C
• PSA: 17.07000
• Density: 1.537g/cm³
• LogP: 3.04180
• Storage Temp.: 2-8°C

Purity/Quality:

97% ^*data from raw suppliers

(3-Bromophenyl)(cyclopropyl)methanone ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-BROMOPHENYL CYCLOPROPYL KETONE

There total 5 articles about 3-BROMOPHENYL CYCLOPROPYL KETONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

(3-bromophenyl)(cyclopropyl)methanol (79134-92-2) → (3-bromophenyl)(cyclopropyl)methanone (693774-26-4)

Guidance literature:

With Dess-Martin periodane; In dichloromethane; at 20 ℃; for 2h;

Reference yield: 70.0%

3-bromobenzoyl chloride (1711-09-7) + cyclopropylmagnesium chloride → (3-bromophenyl)(cyclopropyl)methanone (693774-26-4)

Guidance literature:

With copper(l) chloride; lithium chloride; at -60 ℃;

DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

tricyclopropylbismuthane (925430-09-7) + 1-Bromo-3-iodobenzene (591-18-4) + carbon monoxide (201230-82-2) → (3-bromophenyl)(cyclopropyl)methanone (693774-26-4)

Guidance literature:

With (η3-allyl)(N,N'-bis(2,6-diisopropylphenyl)-4,5-dihydroimidazol-2-ylidene)chloropalladium(II); sodium carbonate; lithium chloride; In N,N-dimethyl-formamide; at 40 ℃; for 16h; under 760.051 Torr; Temperature; Inert atmosphere; Sealed tube;

DOI:10.1055/s-0036-1590832

upstream raw materials:

3-bromobenzoyl chloride

tricyclopropylbismuthane

1-Bromo-3-iodobenzene

carbon monoxide

Downstream raw materials:

5-(3-bromophenyl)-5-cyclopropyl-3-methylimidazolidine-2,4-dione

5-(3-bromophenyl)-5-cyclopropyl-3-methyl-2-thioxoimidazolidin-4-one

5-(3-bromophenyl)-5-cyclopropyl-2-imino-3-methylimidazolidin-4-one

C₁₁H₁₂BrNO₂

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