Methyl 3-(acetylamino)-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

Base Information

• Chemical Name: Methyl 3-(acetylamino)-2,3,6-trideoxy-α-L-lyxo-hexopyranoside
• CAS No.: 32385-07-2
• Molecular Formula: C9H17NO4
• Molecular Weight: 203.24
• Mol file: 32385-07-2.mol

Synonyms:Methyl 3-(acetylamino)-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

Chemical Property of Methyl 3-(acetylamino)-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

Chemical Property:

• PSA: 67.79000
• LogP: 0.02420

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

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Technology Process of Methyl 3-(acetylamino)-2,3,6-trideoxy-α-L-lyxo-hexopyranoside

There total 26 articles about Methyl 3-(acetylamino)-2,3,6-trideoxy-α-L-lyxo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 92.0%

methyl α-L-daunosaminide (18977-92-9) + acetic anhydride (108-24-7) → methyl 3-acetamido-2,3,6-trideoxy-α-L-lyxo-hexopyranoside (32385-07-2)

Guidance literature:

With triethylamine; In dichloromethane; for 0.333333h; Ambient temperature;

DOI:10.1021/ja00291a028

Reference yield: 90.0%

methyl 3-acetamido-2,3,6-trideoxy-α-L-threo-hexopyranosid-4-ulose (89550-37-8,96796-48-4) → methyl 3-acetamido-2,3,6-trideoxy-α-L-lyxo-hexopyranoside (32385-07-2)

Guidance literature:

With L-Selectride; In tetrahydrofuran; at -40 ℃; for 2h;

DOI:10.1016/0008-6215(85)85215-0

Reference yield: 72.0%

2,3,4,6-tetradeoxy-4',5'-dihydro-2'-methyl(methyl α-DL-lyxo-hexopyranosido)<3,4-d>oxazole → methyl 3-acetamido-2,3,6-trideoxy-α-DL-lyxo-hexopyranoside (6605-27-2,17016-62-5,23089-57-8,23089-61-4,32385-07-2,40879-86-5,53626-04-3,57918-56-6,58769-78-1,67693-35-0,67776-31-2,73979-08-5,91517-12-3,91752-71-5,91752-72-6,93253-07-7,93274-51-2,103773-72-4)

Guidance literature:

With pyridine; toluene-4-sulfonic acid; In water; at 100 ℃; for 2h;

upstream raw materials:

methyl α-L-daunosaminide

acetic anhydride

methyl 3-acetamido-2,3,6-trideoxy-α-L-threo-hexopyranosid-4-ulose

2-methyl-(methyl 2,3,4,6-tetradeoxy-α-L-galactopyranosido)-<3,4-d>-2-oxazoline

Downstream raw materials:

methyl 3-acetamido-2,3,6-trideoxy-β-L-lyxo-hexopyranoside

Methyl 4-O-acetyl-3-acetamido-2,3,6-trideoxy-α-L-lyxopyranoside

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