Valerophenone, 3,4-dihydroxy-4-methyl- (8CI)

Base Information

• Chemical Name: Valerophenone, 3,4-dihydroxy-4-methyl- (8CI)
• CAS No.: 26115-81-1
• Molecular Formula: C₁₂H₁₆O₃
• Molecular Weight: 208.257
• Hs Code.: 2914501900
• Mol file: 26115-81-1.mol

Synonyms:Valerophenone, 3,4-dihydroxy-4-methyl- (8CI)

Chemical Property of Valerophenone, 3,4-dihydroxy-4-methyl- (8CI)

Chemical Property:

• PSA: 57.53000
• LogP: 1.39120

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Valerophenone, 3,4-dihydroxy-4-methyl- (8CI)

There total 3 articles about Valerophenone, 3,4-dihydroxy-4-methyl- (8CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 1-(3,4-dihydroxy-phenyl)-4-methyl-pentan-1-one (26115-81-1)

Guidance literature:

With carbon disulfide; aluminium trichloride; und Erhitzen des vom Schwefelkohlenstoff befreiten Rektionsgemisches bis auf 140grad;

DOI:10.1021/ja01268a003

Reference yield:

4-methylvaleroyl chloride (38136-29-7) + benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 1-(3,4-dihydroxy-phenyl)-4-methyl-pentan-1-one (26115-81-1)

Guidance literature:

With aluminium trichloride; In chlorobenzene; at 110 ℃;

Reference yield:

4-methylvaleroyl chloride (38136-29-7) + benzene-1,2-diol (120-80-9,19481-10-8,37349-32-9) → 1-(3,4-dihydroxy-phenyl)-4-methyl-pentan-1-one (26115-81-1)

Guidance literature:

With carbon disulfide; aluminium trichloride; und anschliessend Erhitzen auf 140grad unter Abdestillieren des Schwefelkohlenstoffs;

DOI:10.1021/ja01268a003

upstream raw materials:

4-methylvaleroyl chloride

benzene-1,2-diol

Downstream raw materials:

1-(3,4-Dihydroxy-phenyl)-4-methyl-pentan-1-ol

Refernces