dichloroplatinum(2+) 4-cyanopiperidin-1-ide 4-cyano-2H-pyridin-1-ide (1:1:1)

Base Information

Chemical Name:dichloroplatinum(2+) 4-cyanopiperidin-1-ide 4-cyano-2H-pyridin-1-ide (1:1:1)
CAS No.:14282-15-6
Molecular Formula:C12H14Cl2N4Pt
Molecular Weight:480.2564
Hs Code.:

Synonyms:

Suppliers and Price of dichloroplatinum(2+) 4-cyanopiperidin-1-ide 4-cyano-2H-pyridin-1-ide (1:1:1)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of dichloroplatinum(2+) 4-cyanopiperidin-1-ide 4-cyano-2H-pyridin-1-ide (1:1:1)

Chemical Property:

Vapor Pressure:0.082mmHg at 25°C
Boiling Point:226.4°Cat760mmHg
Flash Point:90.7°C
Density:g/cm³

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of dichloroplatinum(2+) 4-cyanopiperidin-1-ide 4-cyano-2H-pyridin-1-ide (1:1:1)

There total 3 articles about dichloroplatinum(2+) 4-cyanopiperidin-1-ide 4-cyano-2H-pyridin-1-ide (1:1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

: 100-48-1
pyridine-4-carbonitrile

: dichlorobis(dimethyl sulfoxide)platinum(II)

: 14282-15-6,24476-73-1
trans-[Pt^II(4-CNpy)₂Cl₂]

Guidance literature:: In acetonitrile; at 81.2 ℃;
DOI:10.1021/acs.inorgchem.7b01294

Reference yield:

: 100-48-1
pyridine-4-carbonitrile

: 10025-99-7
potassium tetrachloroplatinate(II)

: 24476-73-1,14282-15-6
cis-{Pt(4-CN-py)2Cl2}

Guidance literature:: In water; dissoln. of 2.64 mmol of 4-cyanopyridine in a minimum amount of water; addn. to a stirred soln. of 1.205 mmol K2(PtCl4) in distilled water; stirring for several hours; storing in a refrigerator; pptn.; filtration;; washing twice with ice-water, ice-ethanol and ether; drying in vac. over P2O5; elem. anal.;;
DOI:10.1039/DT9930000233

Reference yield:

: 100-48-1
pyridine-4-carbonitrile

: 10025-99-7
potassium tetrachloroplatinate(II)

: 14282-15-6,24476-73-1
trans-[Pt^II(4-CNpy)₂Cl₂]

Guidance literature:: In N,N-dimethyl-formamide; addn. of 2.1 molar equivalents of 4-cyanopyridine to a soln. of K2(PtCl4) in DMF; keeping at 80°C for 6 h; evaporation of the solvent under reduced pressure;; crystallization of the residue from boiling chloroform; elem. anal.;;
DOI:10.1039/DT9930000233