3-Cyano-N-phenylbenzenesulfonamide

Base Information

• Chemical Name: 3-Cyano-N-phenylbenzenesulfonamide
• CAS No.: 56542-65-5
• Molecular Formula: C13H10N2O2S
• Molecular Weight: 258.301
• Mol file: 56542-65-5.mol

Synonyms:3-Cyano-N-phenylbenzenesulfonamide

Chemical Property of 3-Cyano-N-phenylbenzenesulfonamide

Chemical Property:

• PSA: 78.34000
• LogP: 3.51288
• Storage Temp.: Sealed in dry,Room Temperature

Purity/Quality:

97% ^*data from raw suppliers

3-Cyano-N-phenylbenzenesulfonamide 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-Cyano-N-phenylbenzenesulfonamide

There total 2 articles about 3-Cyano-N-phenylbenzenesulfonamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3-cyanobenzene sulfonyl chloride (56542-67-7) + aniline (62-53-3) → 3-cyano-N-phenyl-benzenesulfonamide (56542-65-5)

Guidance literature:

With pyridine; In dichloromethane; at 20 ℃;

DOI:10.1016/j.bmc.2012.08.042

Reference yield: 53.0%

nitrobenzene (98-95-3,26969-40-4) + (3‐cyanophenyl)boronic acid (150255-96-2) → 3-cyano-N-phenyl-benzenesulfonamide (56542-65-5)

Guidance literature:

With potassium pyrosulfite; tetrabutyl-ammonium chloride; potassium carbonate; In acetonitrile; at 130 ℃; for 36h; Sealed tube;

DOI:10.1021/acs.orglett.0c00183

Reference yield:

3-cyano-N-phenyl-benzenesulfonamide (56542-65-5) → C13H13N3O3S

Guidance literature:

With hydroxylamine hydrochloride; N-ethyl-N,N-diisopropylamine; In ethanol; at 87 ℃; for 1h;

DOI:10.1016/j.bmc.2012.08.042

upstream raw materials:

3-cyanobenzene sulfonyl chloride

aniline

nitrobenzene

(3‐cyanophenyl)boronic acid

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