1-(3-CHLOROISOBUTYL)-1,1,3,3,3-PENTACHLORO-1,3-DISILAPROPANE

Base Information

• Chemical Name: 1-(3-CHLOROISOBUTYL)-1,1,3,3,3-PENTACHLORO-1,3-DISILAPROPANE
• CAS No.: 1627573-20-9
• Molecular Formula: C5H10Cl6Si2
• Molecular Weight: 339.02
• Mol file: 1627573-20-9.mol

Synonyms:1-(3-CHLOROISOBUTYL)-1,1,3,3,3-PENTACHLORO-1,3-DISILAPROPANE

Chemical Property of 1-(3-CHLOROISOBUTYL)-1,1,3,3,3-PENTACHLORO-1,3-DISILAPROPANE

Chemical Property:

• Boiling Point: 89-91°C / 0.4
• PSA: 0.00000
• LogP: 4.97560

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 1-(3-CHLOROISOBUTYL)-1,1,3,3,3-PENTACHLORO-1,3-DISILAPROPANE

There total 2 articles about 1-(3-CHLOROISOBUTYL)-1,1,3,3,3-PENTACHLORO-1,3-DISILAPROPANE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(dichlorosilylmethyl)trichlorosilane (18171-02-3) + 1,1,1,3,3,3-hexachloro-1,3-disilapropane (4142-85-2) + 3-Chloro-2-methylpropene (563-47-3) → 1,1,1,3,3,6-hexachloro-5-methyl-1,3-disilahexane (1627573-20-9)

Guidance literature:

With hexachloroplatinic acid; In tetrahydrofuran; at 110 - 130 ℃; for 3h;

Reference yield: 60.0%

1,1,1,3,3,3-hexachloro-1,3-disilapropane (4142-85-2) + 3-Chloro-2-methylpropene (563-47-3) → 1,1,1,3,3,6-hexachloro-5-methyl-1,3-disilahexane (1627573-20-9)

Guidance literature:

1,1,1,3,3,3-hexachloro-1,3-disilapropane; With trihexyl(tetradecyl)phosphonium chloride; Dichloromethylsilane; at 80 - 90 ℃; for 10h; Inert atmosphere; Autoclave;

3-Chloro-2-methylpropene; With dihydrogen hexachloroplatinate; In tetrahydrofuran; at 110 - 120 ℃; Inert atmosphere;

DOI:10.1002/chem.201402757

Reference yield: 60.0%

1,1,1,3,3,6-hexachloro-5-methyl-1,3-disilahexane (1627573-20-9) + orthoformic acid triethyl ester (122-51-0) → 1,1,1,3,3-pentaethoxy-6-chloro-5-methyl-1,3-disilahexane (1621184-24-4)

Guidance literature:

In water; at 80 - 120 ℃;

upstream raw materials:

1,1,1,3,3,3-hexachloro-1,3-disilapropane

3-Chloro-2-methylpropene

(dichlorosilylmethyl)trichlorosilane

Downstream raw materials:

1,1,1,3,3-pentaethoxy-6-chloro-5-methyl-1,3-disilahexane