tert-Butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate

Base Information

• Chemical Name: tert-Butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate
• CAS No.: 1373223-18-7
• Molecular Formula: C11H12ClF3N2O2
• Molecular Weight: 296.67
• Mol file: 1373223-18-7.mol

Synonyms:tert-Butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate;(2-Chloro-6-trifluoromethyl-pyridin-4-yl)-carbamic acid tert-butyl ester

Chemical Property of tert-Butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate

Chemical Property:

• PSA: 51.22000
• LogP: 4.17380

Purity/Quality:

97% ^*data from raw suppliers

(2-Chloro-6-Trifluoromethyl-Pyridin-4-Yl)-CarbamicAcidTert-ButylEster ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of tert-Butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate

There total 1 articles about tert-Butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 33.0%

di-tert-butyl dicarbonate (24424-99-5) + 4-amino-2-chloro-6-(trifluoromethyl)pyridine (34486-22-1) → tert-butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate (1373223-18-7)

Guidance literature:

With dmap; triethylamine; In tetrahydrofuran; at 25 ℃; for 16h;

Reference yield:

tert-butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate (1373223-18-7) + C13H13BrClNOS → C24H24Cl2F3N3O3S

Guidance literature:

tert-butyl (2-chloro-6-(trifluoromethyl)pyridin-4-yl)carbamate; With sodium hydride; In N,N-dimethyl-formamide; at 0 ℃; for 0.5h;

C₁₃H₁₃BrClNOS; In N,N-dimethyl-formamide; at 20 ℃; for 2h;

upstream raw materials:

di-tert-butyl dicarbonate

4-amino-2-chloro-6-(trifluoromethyl)pyridine

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