4-broMo-3-Methoxypyridine hydrochloride

Base Information

• Chemical Name: 4-broMo-3-Methoxypyridine hydrochloride
• CAS No.: 1209335-53-4
• Molecular Formula: C₆H₆BrNO*ClH
• Molecular Weight: 224.485
• Hs Code.: 2933399090
• Mol file: 1209335-53-4.mol

Synonyms:Pyridine, 4-broMo-3-Methoxy-, hydrochloride

Chemical Property of 4-broMo-3-Methoxypyridine hydrochloride

Chemical Property:

• PSA: 22.12000
• LogP: 2.65470
• Storage Temp.: under inert gas (nitrogen or Argon) at 2-8°C

Purity/Quality:

99%, ^*data from raw suppliers

4-Bromo-3-methoxypyridine hydrochloride 95+% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-broMo-3-Methoxypyridine hydrochloride

There total 2 articles about 4-broMo-3-Methoxypyridine hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

3-methoxy-4-nitropyridine 1-oxide (19355-04-5) → 4-bromo-3-methoxypyridine hydrochloride (1209335-53-4)

Guidance literature:

3-methoxy-4-nitropyridine 1-oxide; With phosphorus tribromide; In ethyl acetate; for 17h; Reflux;

With hydrogenchloride; In diethyl ether; ethyl acetate;

Reference yield:

4-bromo-3-methoxy-pyridine (109911-38-8) → 4-bromo-3-methoxypyridine hydrochloride (1209335-53-4)

Guidance literature:

With hydrogenchloride; In diethyl ether; ethyl acetate;

Reference yield: 56.0%

4-bromo-3-methoxypyridine hydrochloride (1209335-53-4) + 4-tert-Butylphenylacetylene (772-38-3) → 4-((4-(tert-butyl)phenyl)ethynyl)-3-methoxypyridine (1616101-89-3)

Guidance literature:

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triethylamine; In N,N-dimethyl-formamide; at 60 ℃; for 15h; Inert atmosphere;

upstream raw materials:

4-bromo-3-methoxy-pyridine

3-methoxy-4-nitropyridine 1-oxide

Downstream raw materials:

4-((4-(tert-butyl)phenyl)ethynyl)-3-methoxypyridine

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