ST 679

Base Information

Chemical Name:ST 679
CAS No.:104076-16-6
Molecular Formula:C24H24N2O5
Molecular Weight:420.45776
Hs Code.:2933990090
Mol file:104076-16-6.mol

Synonyms:ST 679

Suppliers and Price of ST 679

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of ST 679

Chemical Property:

Boiling Point:663.3oC at 760mmHg
Flash Point:354.9oC
PSA：90.12000
Density:1.19g/cm3
LogP:3.67770

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of ST 679

There total 10 articles about ST 679 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 74.8%

: 90-05-1
2-methoxy-phenol

: 87344-05-6
Tolmetin glycine amide

: 104076-16-6,87344-06-7
amtolmetin guacil

Guidance literature:: With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In dichloromethane; at 25 - 30 ℃; Large scale reaction;
DOI:10.1021/op900284w

Reference yield: 60.0%

: 75368-99-9
amino acetic acid guacil ester hydrochloride

: 26171-23-3
1-methyl-5-(p-toluoyl)pyrrole-2-acetic acid

: 104076-16-6,87344-06-7
amtolmetin guacil

Guidance literature:: With potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide; In acetone; at -5 - 30 ℃; for 5h;
DOI:10.1021/op900284w

Reference yield:

: 96-54-8
N-Methylpyrrole

: 104076-16-6,87344-06-7
amtolmetin guacil

Guidance literature:: Multi-step reaction with 6 steps

1.1: dichloromethane / 1 h / -10 - 0 °C

1.2: 0.5 h / -10 - 0 °C / pH 10

2.1: hydrazine hydrate; potassium hydroxide / water / 5 h / 100 °C

3.1: potassium carbonate / dichloromethane / 3 h / 30 °C

4.1: o-xylene / 24 h / 145 °C

5.1: sodium hydroxide / methanol; water / 2 h / 30 °C

6.1: potassium carbonate; benzotriazol-1-ol; dicyclohexyl-carbodiimide / acetone / 5 h / -5 - 30 °C

With potassium carbonate; benzotriazol-1-ol; hydrazine hydrate; dicyclohexyl-carbodiimide; potassium hydroxide; sodium hydroxide; In methanol; dichloromethane; o-xylene; water; acetone; 2.1: Wolff-Kishner reduction;
DOI:10.1021/op900284w