5-(4-CHLORO-PHENYL)-ISOXAZOLE-3-CARBONYL CHLORIDE

Base Information

• Chemical Name: 5-(4-CHLORO-PHENYL)-ISOXAZOLE-3-CARBONYL CHLORIDE
• CAS No.: 50872-45-2
• Molecular Formula: C10H5Cl2NO2
• Molecular Weight: 242.061
• Hs Code.: 2934999090
• Mol file: 50872-45-2.mol

Synonyms:TIMTEC-BB SBB009529;ASINEX-REAG BAS 13527876;ART-CHEM-BB B020849;5-(4-CHLORO-PHENYL)-ISOXAZOLE-3-CARBONYL CHLORIDE;AKOS B020849

Chemical Property of 5-(4-CHLORO-PHENYL)-ISOXAZOLE-3-CARBONYL CHLORIDE

Chemical Property:

• PSA: 43.10000
• LogP: 3.37400

Purity/Quality:

98%min ^*data from raw suppliers

5-(4-Chloro-phenyl)-isoxazole-3-carbonyl chloride ^*data from reagent suppliers

Safty Information:

• Hazard Codes: Xi

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-(4-CHLORO-PHENYL)-ISOXAZOLE-3-CARBONYL CHLORIDE

There total 1 articles about 5-(4-CHLORO-PHENYL)-ISOXAZOLE-3-CARBONYL CHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

5-(3-chlorophenyl)isoxazole-1-carboxylic acid (33282-22-3) → C10H5Cl2NO2 (50872-45-2)

Guidance literature:

With oxalyl dichloride; In dichloromethane; N,N-dimethyl-formamide; for 2h;

Reference yield: 47.0%

C10H5Cl2NO2 (50872-45-2) + (-)(1Z,4R,5S,6S,7S)-4,5-epoxy-14-hydroxygermacra-1(10),11(13)-dien-12,6-olide → ((3aR,9aR,10aS,10bS,Z)-9a-methyl-3-methylene-2-oxo-2,3,3a,4,5,8,9,9a,10a,10b-decahydrooxireno[2',3':9,10]cyclodeca[1,2-b]furan-6-yl)methyl 5-(4-chlorophenyl)isoxazole-3-carboxylate

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2016.06.028

Reference yield: 47.0%

C10H5Cl2NO2 (50872-45-2) + 9β-hydroxy-4α,5β-epoxycostunolide → (3aR,5S,9aR,10aS,10bS,E)-6,9a-dimethyl-3-methylene-2-oxo-2,3,3a,4,5,8,9,9a,10a,10b-decahydrooxireno[2',3':9,10]cyclodeca[1,2-b]furan-5-yl 5-(4-chlorophenyl)isoxazole-3-carboxylate

Guidance literature:

With dmap; triethylamine; In dichloromethane; at 20 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2016.06.028

upstream raw materials:

5-(3-chlorophenyl)isoxazole-1-carboxylic acid

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