5-BroMo-4-(broMoMethyl)-2-chloropyridine

Base Information

• Chemical Name: 5-BroMo-4-(broMoMethyl)-2-chloropyridine
• CAS No.: 778611-65-7
• Molecular Formula: C6H4Br2ClN
• Molecular Weight: 285.365
• Hs Code.: 2933399090
• Mol file: 778611-65-7.mol

Synonyms:5-bromo-4-bromomethyl-2-chloropyridine;5-Bromo-4,6-dimethyl-nicotinic acid;

Chemical Property of 5-BroMo-4-(broMoMethyl)-2-chloropyridine

Chemical Property:

• PSA: 12.89000
• LogP: 3.39240
• Storage Temp.: 2-8°C

Purity/Quality:

95+% ^*data from raw suppliers

5-bromo-4-(bromomethyl)-2-chloropyridine 95 ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 5-BroMo-4-(broMoMethyl)-2-chloropyridine

There total 1 articles about 5-BroMo-4-(broMoMethyl)-2-chloropyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-amino-5-bromo-4-methylpyridine (98198-48-2) → 5-bromo-4-(bromomethyl)-2-chloropyridine (778611-65-7)

Guidance literature:

Multi-step reaction with 2 steps

1.1: sodium nitrite; concd. hydrochloric acid / 1 h / -20 °C

1.2: 48 percent / aq. sodium hydroxide / 0 - 5 °C / pH 11

2.1: 47 percent / N-bromosuccinimide; benzoyl peroxide / CCl₄ / Heating

With hydrogenchloride; N-Bromosuccinimide; sodium nitrite; dibenzoyl peroxide; In tetrachloromethane;

DOI:10.1002/jhet.5570410414

upstream raw materials:

2-amino-5-bromo-4-methylpyridine

Refernces