(1R,2R)-2-isothiocyanato-N,N-diMethyl- CyclohexanaMin

Base Information

• Chemical Name: (1R,2R)-2-isothiocyanato-N,N-diMethyl- CyclohexanaMin
• CAS No.: 1020665-66-0
• Molecular Formula: C9H16N2S
• Molecular Weight: 184.305
• Mol file: 1020665-66-0.mol

Synonyms:(1R,2R)-2-isothiocyanato-N,N-diMethyl- CyclohexanaMin;(1R,2R)-2-Isothiocyanato-N,N-dimethylcyclohexanamine

Chemical Property of (1R,2R)-2-isothiocyanato-N,N-diMethyl- CyclohexanaMin

Chemical Property:

Purity/Quality:

99% ^*data from raw suppliers

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Technology Process of (1R,2R)-2-isothiocyanato-N,N-diMethyl- CyclohexanaMin

There total 1 articles about (1R,2R)-2-isothiocyanato-N,N-diMethyl- CyclohexanaMin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

thiophosgene (463-71-8) + (1R,2R)-N,N-dimethylcyclohexane-1,2-diamine (320778-92-5) → (1R,2R)-2-isothiocyanato-N,N-dimethylcyclohexanamine (1020665-66-0)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 4h; cooling;

DOI:10.1039/b718949d

Reference yield: 99.0%

N-((1R,2R)-2-amino-1,2-diphenylethyl)-3,5-bis(trifluoromethyl)benzenesulfonamide + (1R,2R)-2-isothiocyanato-N,N-dimethylcyclohexanamine (1020665-66-0) → N-((1R,2R)-2-(3-((1R,2R)-2-(dimethylamino)cyclohexyl)thioureido)-1,2-diphenylethyl)-3,5-bis(trifluoromethyl)benzenesulfonamide (1020665-73-9)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1039/b718949d

Reference yield: 98.0%

(1S,2R)-2-Amino-1,2-diphenylethanol (23364-44-5) + (1R,2R)-2-isothiocyanato-N,N-dimethylcyclohexanamine (1020665-66-0) → 1-((1R,2R)-2-(dimethylamino)cyclohexyl)-3-((1R,2S)-2-hydroxy-1,2-diphenylethyl)thiourea (1046493-36-0)

Guidance literature:

In tetrahydrofuran; at 20 ℃;

DOI:10.1002/chem.200801420

upstream raw materials:

thiophosgene

(1R,2R)-N,N-dimethylcyclohexane-1,2-diamine

Downstream raw materials:

N-((1R,2R)-2-(3-((1R,2R)-2-(dimethylamino)cyclohexyl)thioureido)-1,2-diphenylethyl)-3,5-bis(trifluoromethyl)benzenesulfonamide

N-((1R,2R)-2-(3-((1R,2R)-2-(dimethylamino)cyclohexyl)thioureido)-1,2-diphenylethyl)methanesulfonamide

1-((1R,2R)-2-(N-methyl-N-tosylamino)-1,2-diphenylethyl)-3-((1R,2R)-2-(dimethylamino)cyclohexyl)thiourea

1-((1R,2R)-2-(dimethylamino)cyclohexyl)-3-((1S,2S)-1,2-diphenyl-2-(tosylamino)ethyl)thiourea

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