13-Chlorotridecan-1-ol

Base Information

Chemical Name:13-Chlorotridecan-1-ol
CAS No.:72848-19-2
Molecular Formula:C₁₃H₂₇ClO
Molecular Weight:234.81
Hs Code.:2905590090
DSSTox Substance ID:DTXSID50506108
Nikkaji Number:J25.066J
Wikidata:Q82361691
Mol file:72848-19-2.mol

Synonyms:13-chlorotridecan-1-ol;72848-19-2;SCHEMBL4528431;DTXSID50506108

Suppliers and Price of 13-Chlorotridecan-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 13-Chlorotridecan-1-ol

Chemical Property:

PSA：20.23000
LogP:4.50860
XLogP3:5.4
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:12
Exact Mass:234.1750432
Heavy Atom Count:15
Complexity:107

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C(CCCCCCO)CCCCCCCl

Technology Process of 13-Chlorotridecan-1-ol

There total 3 articles about 13-Chlorotridecan-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 13362-52-2
1,13-tridecanediol

: 72848-19-2
1-chloro-13-hydroxytridecane

Guidance literature:: With hydrogenchloride; In n-heptane; at 95 - 100 ℃; for 3h; during the reaction was the product continuously extracted with heptane;

Reference yield:

: 15423-05-9
diethyl 1,11-undecanedicarboxylate

: 72848-19-2
1-chloro-13-hydroxytridecane

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / H₂ / copper-chromium catalyst / ethanol / 6 h / 250 °C / 114000 Torr

2: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane

With hydrogenchloride; hydrogen; copper chromite; In ethanol; n-heptane;

Reference yield:

: 4017-60-1,75232-70-1
ethyl 2-oxocyclododecane-1-carboxylate

: 72848-19-2
1-chloro-13-hydroxytridecane

Guidance literature:: Multi-step reaction with 3 steps

1: 93.5 percent / ethanol / 14 h / Heating

2: 94 percent / H₂ / copper-chromium catalyst / ethanol / 6 h / 250 °C / 114000 Torr

3: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane

With hydrogenchloride; hydrogen; copper chromite; In ethanol; n-heptane;