Technology Process of 13-Hydroxytridecylmalonic acid
There total 4 articles about 13-Hydroxytridecylmalonic acid which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 94 percent / H2 / copper-chromium catalyst / ethanol / 6 h / 250 °C / 114000 Torr
2: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane
3: 2) potassium hydroxide / 1) ethanol, heated 15 h 2) aq. ethanol, heated 4 h
With
hydrogenchloride; potassium hydroxide; hydrogen;
copper chromite;
In
ethanol; n-heptane;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 93.5 percent / ethanol / 14 h / Heating
2: 94 percent / H2 / copper-chromium catalyst / ethanol / 6 h / 250 °C / 114000 Torr
3: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane
4: 2) potassium hydroxide / 1) ethanol, heated 15 h 2) aq. ethanol, heated 4 h
With
hydrogenchloride; potassium hydroxide; hydrogen;
copper chromite;
In
ethanol; n-heptane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 81 percent / hydrogen chloride / heptane / 3 h / 95 - 100 °C / during the reaction was the product continuously extracted with heptane
2: 2) potassium hydroxide / 1) ethanol, heated 15 h 2) aq. ethanol, heated 4 h
With
hydrogenchloride; potassium hydroxide;
In
n-heptane;
