sodium 4-hydroxy-3,5-dimethylbenzenesulphonate

Base Information

• Chemical Name: sodium 4-hydroxy-3,5-dimethylbenzenesulphonate
• CAS No.: 15205-65-9
• Molecular Formula: C8H10 O4 S . Na
• Molecular Weight: 224.213
• Hs Code.: 2907199090
• Mol file: 15205-65-9.mol

Synonyms:3,5-Xylenesulfonicacid, 4-hydroxy-, monosodium salt (8CI); Benzenesulfonic acid, 4-hydroxy-3,5-dimethyl-,monosodium salt (9CI)

Chemical Property of sodium 4-hydroxy-3,5-dimethylbenzenesulphonate

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 85.81000
• Density: g/cm³
• LogP: 2.77470

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of sodium 4-hydroxy-3,5-dimethylbenzenesulphonate

There total 2 articles about sodium 4-hydroxy-3,5-dimethylbenzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

4-Hydroxy-3,5-dimethyl-benzenesulfonic acid; compound with 4-dimethylaminomethyl-2,6-dimethyl-phenol (115198-18-0) → 4-[(dimethylamino)methyl]-2,6-dimethylphenol (42900-95-8) + sodium 2,6-dimethyl sulfonatophenol (15205-65-9)

Guidance literature:

With sodium hydroxide; In water; for 3h;

DOI:10.1007/BF00958336

Reference yield:

→ sodium 2,6-dimethyl sulfonatophenol (15205-65-9)

Guidance literature:

DOI:10.1002/hlca.19680510830

Reference yield:

sodium 2,6-dimethyl sulfonatophenol (15205-65-9) → Acetic acid 2,6-dimethyl-4-(3-nitro-phenoxysulfonyl)-phenyl ester

Guidance literature:

Multi-step reaction with 3 steps

1: Ambient temperature

2: PCl₅ / H₂O / 0 °C

3: Et₃N / CH₂Cl₂ / Ambient temperature

With phosphorus pentachloride; triethylamine; In dichloromethane; water;

DOI:10.1039/a703645k

upstream raw materials:

4-Hydroxy-3,5-dimethyl-benzenesulfonic acid; compound with 4-dimethylaminomethyl-2,6-dimethyl-phenol

Downstream raw materials:

3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

4-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

4-chloro-2-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

2-chloro-4-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate