3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

Base Information

• Chemical Name: 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate
• CAS No.: 116652-81-4
• Molecular Formula: C₁₄H₁₃NO₆S
• Molecular Weight: 323.326
• Mol file: 116652-81-4.mol

Synonyms:3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

Chemical Property of 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate

There total 4 articles about 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

meta-nitrophenol (554-84-7) → 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate (116652-81-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: HCl / ethanol / 0.5 h / Heating

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;

DOI:10.1039/a703645k

Reference yield:

sodium 2,6-dimethyl sulfonatophenol (15205-65-9) → 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate (116652-81-4)

Guidance literature:

Multi-step reaction with 4 steps

1: Ambient temperature

2: PCl₅ / H₂O / 0 °C

3: Et₃N / CH₂Cl₂ / Ambient temperature

4: HCl / ethanol / 0.5 h / Heating

With hydrogenchloride; phosphorus pentachloride; triethylamine; In ethanol; dichloromethane; water;

DOI:10.1039/a703645k

Reference yield:

Acetic acid 4-chlorosulfonyl-2,6-dimethyl-phenyl ester → 3-nitrophenyl 3,5-dimethyl-4-hydroxybenzenesulphonate (116652-81-4)

Guidance literature:

Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / Ambient temperature

2: HCl / ethanol / 0.5 h / Heating

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;

DOI:10.1039/a703645k

upstream raw materials:

meta-nitrophenol

sodium 2,6-dimethyl sulfonatophenol

Downstream raw materials:

meta-nitrophenol