9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI)

Base Information

Chemical Name:9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI)
CAS No.:401462-17-7
Molecular Formula:C14H14N2
Molecular Weight:210.27436
Hs Code.:2933990090
Mol file:401462-17-7.mol

Synonyms:9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI);1 - Ethyl - 3 - Methyl - 9H - pyrido[3,4 - b]indole;9H-Pyrido[3,4-b]indole, 1-ethyl-3-methyl-

Suppliers and Price of 9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI)

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Crysdot
1-Ethyl-3-methyl-9H-pyrido[3,4-b]indole 95+%
1g
$ 535.00

American Custom Chemicals Corporation
1-ETHYL-3-METHYL-9H-PYRIDO[3,4-B]INDOLE 95.00%
5MG
$ 497.26

Alichem
1-Ethyl-3-methyl-9H-pyrido[3,4-b]indole
1g
$ 436.00

AK Scientific
1-Ethyl-3-methyl-9H-pyrido[3,4-b]indole
1g
$ 881.60

aablocks
1-Ethyl-3-methyl-9h-pyrido[3,4-b]indole 95%
1g
$ 488.00

Total 4 raw suppliers

Chemical Property of 9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI)

Chemical Property:

PSA：28.68000
LogP:3.58690

Purity/Quality:

99% ^*data from raw suppliers

1-Ethyl-3-methyl-9H-pyrido[3,4-b]indole 95+% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI)

There total 2 articles about 9H-Pyrido[3,4-b]indole,1-ethyl-3-methyl-(9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 1015760-82-3
(E)-N-(2-(3-oxobut-1-en-1-yl)phenyl)benzenesulfonamide

: 816-40-0
1-Bromo-2-butanone

: 401462-17-7
1-ethyl-3-methyl-9H-pyrido[3,4-b]indole

Guidance literature:: (E)-N-(2-(3-oxobut-1-en-1-yl)phenyl)benzenesulfonamide; 1-Bromo-2-butanone; With triethylamine; In acetonitrile; at 60 ℃; for 0.5h; Schlenk technique;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; at 60 ℃; for 0.5h; Schlenk technique;

With ammonium acetate; In acetonitrile; at 60 ℃; for 12h; Schlenk technique;
DOI:10.1016/j.tetlet.2020.151597

Reference yield:

: 151721-32-3
N-benzenesulfonyl-o-aminobenzaldehyde

: 401462-17-7
1-ethyl-3-methyl-9H-pyrido[3,4-b]indole

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium hydroxide / ethanol; water / 24 h / 20 °C

2.1: triethylamine / acetonitrile / 0.5 h / 60 °C / Schlenk technique

2.2: 0.5 h / 60 °C / Schlenk technique

2.3: 12 h / 60 °C / Schlenk technique

With triethylamine; sodium hydroxide; In ethanol; water; acetonitrile;
DOI:10.1016/j.tetlet.2020.151597