3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE

Base Information

• Chemical Name: 3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE
• CAS No.: 91969-32-3
• Molecular Formula: C11H14O
• Molecular Weight: 162.232
• Hs Code.: 2909309090
• Mol file: 91969-32-3.mol

Synonyms:3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE

Chemical Property of 3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE

Chemical Property:

• Vapor Pressure: 0.179mmHg at 25°C
• Boiling Point: 219.1°C at 760 mmHg
• Flash Point: 80°C
• PSA: 9.23000
• Density: 0.931g/cm³
• LogP: 2.81380

Purity/Quality:

97% ^*data from raw suppliers

3-(2-Methoxyphenyl)-2-methyl-1-propene 97% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE

There total 6 articles about 3-(2-METHOXYPHENYL)-2-METHYL-1-PROPENE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

methallyl acetate (820-71-3) + 2-bromoanisole (578-57-4) → 1-methoxy-2-(2-methylallyl)benzene (91969-32-3)

Guidance literature:

With pyridine; nickel(II) iodide; 4-chloro-2-(4,5-dihydro-1H-imidazol-2-yl)pyridine; tetrabutylammomium bromide; magnesium chloride; zinc; In N,N-dimethyl acetamide; at 60 ℃; for 12h; regioselective reaction; Schlenk technique; Inert atmosphere;

DOI:10.1039/c3ob40232k

Reference yield:

methylallyl phenyl ether (5820-22-4) → 1-methoxy-2-(2-methylallyl)benzene (91969-32-3)

Guidance literature:

Multi-step reaction with 2 steps

2: aqueous NaOH

With sodium hydroxide;

Reference yield:

phenol (108-95-2,27073-41-2) → 1-methoxy-2-(2-methylallyl)benzene (91969-32-3)

Guidance literature:

Multi-step reaction with 3 steps

1: K₂CO₃; acetone

3: aqueous NaOH

With sodium hydroxide; potassium carbonate; acetone;

upstream raw materials:

dimethyl sulfate

2-(methylallyl)phenol

2-bromoanisole

3-Chloro-2-methylpropene

Downstream raw materials:

1-isobutyl-2-methoxybenzene