Technology Process of Methyl 3-[8,18-bis(2-methoxy-2-oxoethyl)-7,12,17-tris(3-methoxy-3-oxopropyl)-3,13-dimethyl-22,24-dihydroporphyrin-2-yl]propanoate
There total 8 articles about Methyl 3-[8,18-bis(2-methoxy-2-oxoethyl)-7,12,17-tris(3-methoxy-3-oxopropyl)-3,13-dimethyl-22,24-dihydroporphyrin-2-yl]propanoate which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2-methylbutanedioic acid;
In
acetic acid;
for 5h;
DOI:10.1039/P19870000277
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 78 percent / toluene-p-sulphonic acid monohydrate / methanol / 3 h / Heating
2: 1.) H2; 2.) bromine / 1.) palladium charcol (10percent) / 1.) ethanol,20 deg C, 760 mmHg; 2.) acetic acid, 100 deg C, 30 min
3: 11 percent / molten methylsuccinic acid / acetic acid / 5 h
With
2-methylbutanedioic acid; hydrogen; bromine; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
methanol; acetic acid;
DOI:10.1039/P19870000277
- Guidance literature:
-
Multi-step reaction with 4 steps
2: 78 percent / toluene-p-sulphonic acid monohydrate / methanol / 3 h / Heating
3: 1.) H2; 2.) bromine / 1.) palladium charcol (10percent) / 1.) ethanol,20 deg C, 760 mmHg; 2.) acetic acid, 100 deg C, 30 min
4: 11 percent / molten methylsuccinic acid / acetic acid / 5 h
With
2-methylbutanedioic acid; hydrogen; bromine; toluene-4-sulfonic acid;
palladium on activated charcoal;
In
methanol; acetic acid;
DOI:10.1039/P19870000277
