2-(2-nitrophenoxy)benzaldehyde

Base Information

• Chemical Name: 2-(2-nitrophenoxy)benzaldehyde
• CAS No.: 66961-19-1
• Molecular Formula: C13H9NO4
• Molecular Weight: 243.219
• Hs Code.: 2913000090
• Mol file: 66961-19-1.mol

Synonyms:CHEMBRDG-BB 5144034;2-(2-NITROPHENOXY)BENZALDEHYDE;2-(2-nitrophenoxy)benzaldehyde(SALTDATA: FREE)

Chemical Property of 2-(2-nitrophenoxy)benzaldehyde

Chemical Property:

• Vapor Pressure: 1.94E-05mmHg at 25°C
• Boiling Point: 362.4°C at 760 mmHg
• Flash Point: 159.6°C
• PSA: 72.12000
• Density: 1.325g/cm³
• LogP: 3.72280

Purity/Quality:

99% ^*data from raw suppliers

2-(2-nitrophenoxy)benzaldehyde 95% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-(2-nitrophenoxy)benzaldehyde

There total 5 articles about 2-(2-nitrophenoxy)benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

salicylaldehyde (90-02-8) + ortho-nitrofluorobenzene (1493-27-2,127723-77-7) → 2-(2-nitrophenoxy)benzaldehyde (66961-19-1)

Guidance literature:

With potassium carbonate; In N,N-dimethyl-formamide; at 100 ℃; Inert atmosphere;

DOI:10.1002/anie.201610203

Reference yield: 54.0%

ortho-bromobenzaldehyde (6630-33-7) + 2-hydroxynitrobenzene (88-75-5,78813-12-4) → 2-(2-nitrophenoxy)benzaldehyde (66961-19-1)

Guidance literature:

With copper(II) oxide; potassium hydroxide; In N,N-dimethyl acetamide; at 27 ℃; for 24h; Inert atmosphere; Sealed tube;

DOI:10.1016/j.tetlet.2013.01.063

Reference yield:

2-Chloronitrobenzene (88-73-3) → 2-(2-nitrophenoxy)benzaldehyde (66961-19-1)

Guidance literature:

at 170 ℃; weiteres Erhitzen auf 190-200grad;

DOI:10.1021/ja01316a035

upstream raw materials:

2-Chloronitrobenzene

sodium salicylate

ortho-bromobenzaldehyde

2-hydroxynitrobenzene

Downstream raw materials:

2-carboxy-2'-nitrodiphenyl ether

2-amino-5-[2-(2-nitrophenoxy)phenyl]-1,3,4-oxadiazole

10H-dibenzo[b,f][1,4]oxazepin-11-one

2-(2'-aminophenoxy)benzenecarboxylic acid