2-Hydroxy-2'-nitrobenzophenone

Base Information

Chemical Name:2-Hydroxy-2'-nitrobenzophenone
CAS No.:22293-32-9
Molecular Formula:C₁₃H₉NO₄
Molecular Weight:243.219
Hs Code.:
DSSTox Substance ID:DTXSID901270528
Nikkaji Number:J1.440.340J

Synonyms:(2-hydroxyphenyl)(2-nitrophenyl)methanone;22293-32-9;2-Hydroxy-2'-nitrobenzophenone;SCHEMBL11282500;DTXSID901270528

Suppliers and Price of 2-Hydroxy-2'-nitrobenzophenone

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemical Property of 2-Hydroxy-2'-nitrobenzophenone

Chemical Property:

XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:243.05315777
Heavy Atom Count:18
Complexity:325

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C(=C1)C(=O)C2=CC=CC=C2O)[N+](=O)[O-]

Technology Process of 2-Hydroxy-2'-nitrobenzophenone

There total 7 articles about 2-Hydroxy-2'-nitrobenzophenone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 66961-19-1
2-(2-nitrophenoxy)benzaldehyde

: 22293-32-9
(2-hydroxyphenyl)(2-nitrophenyl)methanone

Guidance literature:: With 2-(2,6-dimethoxyphenyl)-2,5,6,7-tetrahydropyrrolo[2,1-c][1,2,4]triazol-4-ium chloride; sodium acetate; In tetrahydrofuran; at 80 ℃; for 4h; Inert atmosphere; Glovebox;
DOI:10.1002/anie.201610203

Reference yield: 40.0%

: 329235-22-5
2-formylphenyl 2-nitrobenzenesulfonate

: 22293-32-9
(2-hydroxyphenyl)(2-nitrophenyl)methanone

Guidance literature:: With di-tert-butyl peroxide; In chlorobenzene; for 24h; Heating;
DOI:10.1016/S0040-4039(00)01746-9

Reference yield:

: 89-95-2
2-methyl-benzyl alcohol

: 22293-32-9
(2-hydroxyphenyl)(2-nitrophenyl)methanone

Guidance literature:: Multi-step reaction with 2 steps

1: 76 percent / NaOH / H₂O; CH₂Cl₂ / 20 °C

2: 40 percent / di-tert-butyl peroxide / chlorobenzene / 24 h / Heating

With sodium hydroxide; di-tert-butyl peroxide; In dichloromethane; water; chlorobenzene;
DOI:10.1016/S0040-4039(00)01746-9