6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester

Base Information

Chemical Name:6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester
CAS No.:4712-73-6
Molecular Formula:C18H18O6
Molecular Weight:330.337
Hs Code.:
Mol file:4712-73-6.mol

Synonyms:6,6'-Dimethoxy-3,3'-biphenyldicarboxylic acid dimethyl ester;6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester

Suppliers and Price of 6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester

Chemical Property:

PSA：71.06000
LogP:2.94400

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester

There total 2 articles about 6,6'-Dimethoxybiphenyl-3,3'-dicarboxylic acid dimethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 269410-10-8
methyl 4-methoxy-3-(4,4,5,5-tetramethyl-1,3,2-dioxaborolan-2-yl)benzoate

: 35387-93-0
3-iodo-4-methoxy-benzoic acid methyl ester

: 4712-73-6
dimethyl 6,6'-dimethoxybiphenyl-3,3'-dicarboxylate

Guidance literature:: With (1,1'-bis(diphenylphosphino)ferrocene)palladium(II) dichloride; potassium carbonate; In 1,4-dioxane; at 20 - 90 ℃; for 14h;
DOI:10.1021/jm200553w

Reference yield:

: 35387-93-0
3-iodo-4-methoxy-benzoic acid methyl ester

: 4712-73-6
dimethyl 6,6'-dimethoxybiphenyl-3,3'-dicarboxylate

Guidance literature:: With copper; at 260 ℃;
DOI:10.1017/S0714980800000659

Reference yield:

: 4712-73-6
dimethyl 6,6'-dimethoxybiphenyl-3,3'-dicarboxylate

: 1806-29-7
2,2'-dihydroxybiphenyl

Guidance literature:: Multi-step reaction with 2 steps

1: aqueous hydriodic acid

2: concentrated aqueous HCl / 270 °C

With hydrogenchloride; hydrogen iodide;
DOI:10.1017/S0714980800000659