3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl-

Base Information

Chemical Name:3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl-
CAS No.:4357-56-6
Molecular Formula:C₈H₆ClNO₅
Molecular Weight:231.592
Hs Code.:2933399090
Mol file:4357-56-6.mol

Synonyms:3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl-

Suppliers and Price of 3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl-

Chemical Property:

PSA：107.72000
LogP:1.14540

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl-

There total 6 articles about 3,4-Pyridinedicarboxylic acid, 2-chloro-5-hydroxy-6-methyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 90110-24-0
3-amino-6-chloro-2-methylpyridin-4,5-dicarboxylic acid

: 4357-56-6
2-chloro-5-hydroxy-6-methyl-pyridine-3,4-dicarboxylic acid

Guidance literature:: With water; sodium nitrite; at 70 ℃;
DOI:10.1021/ja01556a021

Reference yield:

: 18724-73-7
methyl 3-cyano-2-hydroxy-6-methyl-isonicotinate

: 4357-56-6
2-chloro-5-hydroxy-6-methyl-pyridine-3,4-dicarboxylic acid

Guidance literature:: Multi-step reaction with 5 steps

1: urea; acetic acid anhydride; HNO₃

2: chlorobenzene; PCl₅

3: iron; acetic acid

4: platinum; aqueous HCl / Hydrogenation

5: H₂O; aqueous NaNO₂ / 70 °C

With hydrogenchloride; phosphorus pentachloride; water; nitric acid; acetic anhydride; iron; acetic acid; chlorobenzene; urea; platinum; sodium nitrite;
DOI:10.1021/ja01556a021

Reference yield:

: 98590-00-2
3-cyano-2-hydroxy-6-methyl-5-nitro-isonicotinic acid methyl ester

: 4357-56-6
2-chloro-5-hydroxy-6-methyl-pyridine-3,4-dicarboxylic acid

Guidance literature:: Multi-step reaction with 4 steps

1: chlorobenzene; PCl₅

2: iron; acetic acid

3: platinum; aqueous HCl / Hydrogenation

4: H₂O; aqueous NaNO₂ / 70 °C

With hydrogenchloride; phosphorus pentachloride; water; iron; acetic acid; chlorobenzene; platinum; sodium nitrite;
DOI:10.1021/ja01556a021